1-(hydroxymethyl)-14-phenyl-6,13-diazadispiro[4.1.5.2]tetradec-13-en-6-oxyl

Base Information

Chemical Name:1-(hydroxymethyl)-14-phenyl-6,13-diazadispiro[4.1.5.2]tetradec-13-en-6-oxyl
CAS No.:1601419-61-7
Molecular Formula:C₁₉H₂₅N₂O₂
Molecular Weight:313.42
Hs Code.:

Synonyms:1-(hydroxymethyl)-14-phenyl-6,13-diazadispiro[4.1.5.2]tetradec-13-en-6-oxyl

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Chemical Property of 1-(hydroxymethyl)-14-phenyl-6,13-diazadispiro[4.1.5.2]tetradec-13-en-6-oxyl

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Technology Process of 1-(hydroxymethyl)-14-phenyl-6,13-diazadispiro[4.1.5.2]tetradec-13-en-6-oxyl

There total 4 articles about 1-(hydroxymethyl)-14-phenyl-6,13-diazadispiro[4.1.5.2]tetradec-13-en-6-oxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1601419-52-6
(14-phenyl-6,13-diazadispiro[4.1.5.2]tetradec-13-en-1-yl)methanol

: 1601419-61-7
1-(hydroxymethyl)-14-phenyl-6,13-diazadispiro[4.1.5.2]tetradec-13-en-6-oxyl

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at -10 ℃;
DOI:10.1002/pola.27071

Reference yield:

: 1601419-34-4
2-(pent-4-enyl)-3-phenyl-1,4-diazaspiro[4.5]deca-1,3-diene 1-oxide

: 1601419-61-7
1-(hydroxymethyl)-14-phenyl-6,13-diazadispiro[4.1.5.2]tetradec-13-en-6-oxyl

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / Heating

2: edetate disodium; zinc; acetic acid / ethanol / 3 h / 60 °C

3: 3-chloro-benzenecarboperoxoic acid / chloroform / -10 °C

With edetate disodium; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; In ethanol; chloroform; toluene;
DOI:10.1002/pola.27071

Reference yield:

: 1601419-42-4
1’-phenyl-6a’,7’,8’,9’-tetrahydro-6’H-spiro[cyclohexane-1,3’-cyclopenta[c]imidazo[1,5-b]isoxazole]

: 1601419-61-7
1-(hydroxymethyl)-14-phenyl-6,13-diazadispiro[4.1.5.2]tetradec-13-en-6-oxyl

Guidance literature:: Multi-step reaction with 2 steps

1: edetate disodium; zinc; acetic acid / ethanol / 3 h / 60 °C

2: 3-chloro-benzenecarboperoxoic acid / chloroform / -10 °C

With edetate disodium; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; In ethanol; chloroform;
DOI:10.1002/pola.27071