N-(3-(4-methoxyphenyl)prop-2-yn-1-yl)-4-methyl-N-(penta-1,4-dien-3-yl)benzenesulfonamide

Base Information

Chemical Name:N-(3-(4-methoxyphenyl)prop-2-yn-1-yl)-4-methyl-N-(penta-1,4-dien-3-yl)benzenesulfonamide
CAS No.:1312037-32-3
Molecular Formula:C₂₂H₂₃NO₃S
Molecular Weight:381.496
Hs Code.:

Synonyms:N-(3-(4-methoxyphenyl)prop-2-yn-1-yl)-4-methyl-N-(penta-1,4-dien-3-yl)benzenesulfonamide

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Chemical Property of N-(3-(4-methoxyphenyl)prop-2-yn-1-yl)-4-methyl-N-(penta-1,4-dien-3-yl)benzenesulfonamide

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Technology Process of N-(3-(4-methoxyphenyl)prop-2-yn-1-yl)-4-methyl-N-(penta-1,4-dien-3-yl)benzenesulfonamide

There total 2 articles about N-(3-(4-methoxyphenyl)prop-2-yn-1-yl)-4-methyl-N-(penta-1,4-dien-3-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 37614-59-8
4-(4-methoxyphenyl)prop-2-yn-1-ol

: 1312037-35-6
C₁₂H₁₅NO₂S

: 1312037-32-3
N-(3-(4-methoxyphenyl)prop-2-yn-1-yl)-4-methyl-N-(penta-1,4-dien-3-yl)benzenesulfonamide

Guidance literature:: With di-isopropyl azodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/adsc.201000904

Reference yield:

: 40597-41-9
ethyl N-tosylformimidate

: 1312037-32-3
N-(3-(4-methoxyphenyl)prop-2-yn-1-yl)-4-methyl-N-(penta-1,4-dien-3-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 12 h / 20 °C

2: di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

With di-isopropyl azodicarboxylate; In tetrahydrofuran;
DOI:10.1002/adsc.201000904

Reference yield: 55.0%

: 1312037-32-3
N-(3-(4-methoxyphenyl)prop-2-yn-1-yl)-4-methyl-N-(penta-1,4-dien-3-yl)benzenesulfonamide

: 1312037-40-3
6-(4-methoxyphenyl)-3-(p-toluenesulfonyl)-2-vinyl-3-azabicyclo[4.1.0]hept-4-ene

Guidance literature:: With silver(I) tetrafluoroborate; C₃₉H₃₃IN₂PPt; In toluene; at 60 ℃; for 20h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201000904