(2-(2-(benzyloxycarbonylamino)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate

Base Information

Chemical Name:(2-(2-(benzyloxycarbonylamino)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate
CAS No.:1382355-04-5
Molecular Formula:C₇H₇O₃S*C₂₂H₂₀FINO₂
Molecular Weight:647.506
Hs Code.:

Synonyms:(2-(2-(benzyloxycarbonylamino)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate

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Chemical Property of (2-(2-(benzyloxycarbonylamino)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate

Chemical Property:

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Technology Process of (2-(2-(benzyloxycarbonylamino)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate

There total 4 articles about (2-(2-(benzyloxycarbonylamino)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 352-34-1
4-fluoro-1-iodobenzene

: 1382355-04-5
(2-(2-(benzyloxycarbonylamino)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium periodate; acetic anhydride / acetic acid / 2 h / 120 °C

2: dichloromethane; acetonitrile / 1 h / 20 °C / Inert atmosphere

3: dichloromethane; acetonitrile / 24 h / 20 °C / Inert atmosphere

With sodium periodate; acetic anhydride; In dichloromethane; acetic acid; acetonitrile;
DOI:10.1021/jo300874m

Reference yield:

: 1382354-90-6
benzyl 2-(trimethylstannyl)phenylethylcarbamate

: 84383-77-7
(4-fluorophenyl)(hydroxy)-λ3-iodaneyl 4-methylbenzenesulfonate

: 1382355-04-5
(2-(2-(benzyloxycarbonylamino)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate

Guidance literature:: In dichloromethane; acetonitrile; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo300874m

Reference yield:

: 16308-15-9
(4-fluorophenyl)-λ³-iodanediyl diacetate

: 1382355-04-5
(2-(2-(benzyloxycarbonylamino)ethyl)phenyl)(4-fluorophenyl)iodonium p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane; acetonitrile / 1 h / 20 °C / Inert atmosphere

2: dichloromethane; acetonitrile / 24 h / 20 °C / Inert atmosphere

In dichloromethane; acetonitrile;
DOI:10.1021/jo300874m