3-(2-methoxy-5,6,7,8-tetrahydronaphthalen-1-yl)propynoic acid benzyl(cyclohex-1-enyl)amide

Base Information

• Chemical Name: 3-(2-methoxy-5,6,7,8-tetrahydronaphthalen-1-yl)propynoic acid benzyl(cyclohex-1-enyl)amide
• CAS No.: 1140972-74-2
• Molecular Formula: C₂₇H₂₉NO₂
• Molecular Weight: 399.533

Synonyms:3-(2-methoxy-5,6,7,8-tetrahydronaphthalen-1-yl)propynoic acid benzyl(cyclohex-1-enyl)amide

Chemical Property of 3-(2-methoxy-5,6,7,8-tetrahydronaphthalen-1-yl)propynoic acid benzyl(cyclohex-1-enyl)amide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of 3-(2-methoxy-5,6,7,8-tetrahydronaphthalen-1-yl)propynoic acid benzyl(cyclohex-1-enyl)amide

There total 1 articles about 3-(2-methoxy-5,6,7,8-tetrahydronaphthalen-1-yl)propynoic acid benzyl(cyclohex-1-enyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzylcyclohexylimine (4471-09-4) + C14H13ClO2 → 3-(2-methoxy-5,6,7,8-tetrahydronaphthalen-1-yl)propynoic acid benzyl(cyclohex-1-enyl)amide (1140972-74-2)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/ol900373z

Reference yield: 89.0%

3-(2-methoxy-5,6,7,8-tetrahydronaphthalen-1-yl)propynoic acid benzyl(cyclohex-1-enyl)amide (1140972-74-2) → (-)-1-benzyl-4-(2-methoxy-5,6,7,8-tetrahydronaphthalen-1-yl)-5,6,7,8-tetrahydro-1H-quinolin-2-one

Guidance literature:

With (S)-5,5 ′-bis[di(3,5-xylyl)phosphino]-4,4 ′-bi-1,3-benzodioxole; tetrakis(acetonitrile)palladium(II) tetrafluoroborate; In dichloromethane; at 20 ℃; for 72h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1021/ol900373z

upstream raw materials:

N-benzylcyclohexylimine

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