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Technology Process of C24H35P

C24H35P

Base Information
  • Chemical Name:C24H35P
  • CAS No.:1622887-11-9
  • Molecular Formula:C24H35P
  • Molecular Weight:354.516
  • Hs Code.:
C<sub>24</sub>H<sub>35</sub>P

Synonyms:C24H35P

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Chemical Property of C24H35P
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Technology Process of C24H35P

There total 3 articles about C24H35P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

C<sub>16</sub>H<sub>27</sub>LiO

C16H27LiO

C<sub>24</sub>H<sub>35</sub>P
1622887-11-9

C24H35P

Guidance literature:
C16H27LiO; With phosphorus trichloride; In diethyl ether; at 0 - 20 ℃; for 16h;
With lithium aluminium tetrahydride; In diethyl ether; for 3h;
DOI:10.1002/anie.201308002

Reference yield:

C<sub>24</sub>H<sub>34</sub>P<sup>(1-)</sup>*Na<sup>(1+)</sup>

C24H34P(1-)*Na(1+)

C<sub>24</sub>H<sub>35</sub>P
1622887-11-9

C24H35P

C<sub>48</sub>H<sub>68</sub>P<sub>2</sub>

C48H68P2

C<sub>48</sub>H<sub>68</sub>AsClP<sub>2</sub>

C48H68AsClP2

Guidance literature:
With arsenic trichloride; In tetrahydrofuran; at -78 ℃; for 1h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201905922

Reference yield:

2-bromo-1,3-diisopropylbenzene
57190-17-7

2-bromo-1,3-diisopropylbenzene

C<sub>24</sub>H<sub>35</sub>P
1622887-11-9

C24H35P

Guidance literature:
Multi-step reaction with 2 steps
1.1: n-butyllithium / hexane / 26 h / -20 - -10 °C
2.1: phosphorus trichloride / diethyl ether / 16 h / 0 - 20 °C
2.2: 3 h
With n-butyllithium; phosphorus trichloride; In diethyl ether; hexane;
DOI:10.1002/anie.201308002
upstream raw materials:

2-bromo-1,3-diisopropylbenzene

Downstream raw materials:

C48H68GeP2

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