2-(1-bromo-2-(4-fluorophenyl)vinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(1-bromo-2-(4-fluorophenyl)vinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1584694-27-8
Molecular Formula:C₁₄H₁₇BBrFO₂
Molecular Weight:327.001
Hs Code.:

Synonyms:2-(1-bromo-2-(4-fluorophenyl)vinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(1-bromo-2-(4-fluorophenyl)vinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(1-bromo-2-(4-fluorophenyl)vinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about 2-(1-bromo-2-(4-fluorophenyl)vinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 2-(2-(4-fluorophenyl)ethynyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1584694-27-8
2-(1-bromo-2-(4-fluorophenyl)vinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 2-(2-(4-fluorophenyl)ethynyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; With Schwartz's reagent; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

With N-Bromosuccinimide; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2014.02.065

Reference yield:

: 1584694-27-8
2-(1-bromo-2-(4-fluorophenyl)vinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1065498-70-5
2-(2-(4-fluorophenyl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With C₃₀H₄₀IrNO₂P⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-); hydrogen; In dichloromethane; at 50 ℃; for 18h; under 22502.3 Torr; Reagent/catalyst;
DOI:10.1016/j.tet.2014.02.065

Reference yield:

: 1584694-27-8
2-(1-bromo-2-(4-fluorophenyl)vinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1065498-70-5
2-(2-(4-fluorophenyl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1584694-39-2
C₁₄H₁₉BBrFO₂

Guidance literature:: With 1,5-cyclooctadiene{[dibenzyl((4S,5S)-5-methyl-2-phenyl-4,5-dihydro-4-oxazolyl)methyl]dicyclohexylphosphinite κN:κP}iridium(I) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate; hydrogen; In dichloromethane; at 50 ℃; for 18h; under 22502.3 Torr;
DOI:10.1016/j.tet.2014.02.065