1-methyl-2-(4-methoxyphenyl)-3,4-bis<<(N-2-propylcarbamoyl)oxy>methyl>pyrrole

Base Information

Chemical Name:1-methyl-2-(4-methoxyphenyl)-3,4-bis<<(N-2-propylcarbamoyl)oxy>methyl>pyrrole
CAS No.:104156-63-0
Molecular Formula:C₂₂H₃₁N₃O₅
Molecular Weight:417.505
Hs Code.:

Synonyms:1-methyl-2-(4-methoxyphenyl)-3,4-bis<<(N-2-propylcarbamoyl)oxy>methyl>pyrrole

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Chemical Property of 1-methyl-2-(4-methoxyphenyl)-3,4-bis<<(N-2-propylcarbamoyl)oxy>methyl>pyrrole

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Technology Process of 1-methyl-2-(4-methoxyphenyl)-3,4-bis<<(N-2-propylcarbamoyl)oxy>methyl>pyrrole

There total 5 articles about 1-methyl-2-(4-methoxyphenyl)-3,4-bis<<(N-2-propylcarbamoyl)oxy>methyl>pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 104156-62-9
1-methyl-2-(4-methoxyphenyl)-3,4-bis(hydroxymethyl)pyrrole

: 1795-48-8
Isopropyl isocyanate

: 104156-63-0
1-methyl-2-(4-methoxyphenyl)-3,4-bis<<(N-2-propylcarbamoyl)oxy>methyl>pyrrole

Guidance literature:: With dibutyltin diacetate; In dichloromethane; for 15h; Heating;
DOI:10.1021/jm00161a019

Reference yield:

: 104-01-8
4-Methoxyphenylacetic acid

: 104156-63-0
1-methyl-2-(4-methoxyphenyl)-3,4-bis<<(N-2-propylcarbamoyl)oxy>methyl>pyrrole

Guidance literature:: Multi-step reaction with 5 steps

1: N-bromosuccinimide (NBS), 2,2'-azobis(2-methylpropanenitrile) / CCl₄ / 15 h / 35 °C / Irradiation

2: H₂O / 18 h / 65 °C

3: Ac₂O / 1.) 25 deg C, 18 h, 2.) 65 deg C, 4 h

4: 93 percent / lithium aluminum hydride / tetrahydrofuran / 15 h / 25 °C

5: 86 percent / dibutyltin diacetate / CH₂Cl₂ / 15 h / Heating

With N-Bromosuccinimide; lithium aluminium tetrahydride; dibutyltin diacetate; 2,2'-azobis(isobutyronitrile); acetic anhydride; In tetrahydrofuran; tetrachloromethane; dichloromethane; water;
DOI:10.1021/jm00161a019

Reference yield:

: 91012-98-5
(4-methoxyphenyl)(methylamino)acetic acid

: 104156-63-0
1-methyl-2-(4-methoxyphenyl)-3,4-bis<<(N-2-propylcarbamoyl)oxy>methyl>pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: Ac₂O / 1.) 25 deg C, 18 h, 2.) 65 deg C, 4 h

2: 93 percent / lithium aluminum hydride / tetrahydrofuran / 15 h / 25 °C

3: 86 percent / dibutyltin diacetate / CH₂Cl₂ / 15 h / Heating

With lithium aluminium tetrahydride; dibutyltin diacetate; acetic anhydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00161a019