[1-((E)-Propenyl)-6-(tetrahydro-pyran-2-yloxy)-hexyl]-phosphonic acid diethyl ester

Base Information

Chemical Name:[1-((E)-Propenyl)-6-(tetrahydro-pyran-2-yloxy)-hexyl]-phosphonic acid diethyl ester
CAS No.:73881-11-5
Molecular Formula:C₁₈H₃₅O₅P
Molecular Weight:362.447
Hs Code.:

Synonyms:[1-((E)-Propenyl)-6-(tetrahydro-pyran-2-yloxy)-hexyl]-phosphonic acid diethyl ester

Suppliers and Price of [1-((E)-Propenyl)-6-(tetrahydro-pyran-2-yloxy)-hexyl]-phosphonic acid diethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of [1-((E)-Propenyl)-6-(tetrahydro-pyran-2-yloxy)-hexyl]-phosphonic acid diethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of [1-((E)-Propenyl)-6-(tetrahydro-pyran-2-yloxy)-hexyl]-phosphonic acid diethyl ester

There total 1 articles about [1-((E)-Propenyl)-6-(tetrahydro-pyran-2-yloxy)-hexyl]-phosphonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37935-47-0
2-(5-bromopentyloxy)tetrahydropyran

: 26327-86-6
diethyl (E)-crotylphosphonate

: 108-24-7
acetic anhydride

: 55305-36-7
2-((E)-non-6-enyloxy)-tetrahydro-2H-pyran

: 31502-19-9
(E)-6-nonen-1-ol

: 30412-53-4
(E)-6-Nonen-1-yl acetate

: 73881-11-5
[1-((E)-Propenyl)-6-(tetrahydro-pyran-2-yloxy)-hexyl]-phosphonic acid diethyl ester

Guidance literature:: Product distribution; Multistep reaction; A Stereoselective Synthesis of (E)-Olefinic Sex Pheromones of Moths; var. allyl diethyl phosphonates, var. ω-bromoalkyltetrahydropyranyl ethers;
DOI:10.1002/cber.19801130330

Reference yield:

: 73881-11-5
[1-((E)-Propenyl)-6-(tetrahydro-pyran-2-yloxy)-hexyl]-phosphonic acid diethyl ester

: 31502-19-9
(E)-6-nonen-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 1 h / 0 °C

2: p-toluenesulfonic acid / methanol; H₂O / 3 h / Heating

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In methanol; diethyl ether; water;
DOI:10.1002/cber.19801130330