diethyl [1-({[(3R,5S,8S)-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1⁽²³⁾,17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonate

Base Information

• Chemical Name: diethyl [1-({[(3R,5S,8S)-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1⁽²³⁾,17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonate
• CAS No.: 1021488-44-7
• Molecular Formula: C₄₀H₅₇N₄O₉P
• Molecular Weight: 768.888

Synonyms:diethyl [1-({[(3R,5S,8S)-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1⁽²³⁾,17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonate

Chemical Property of diethyl [1-({[(3R,5S,8S)-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1⁽²³⁾,17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonate

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Technology Process of diethyl [1-({[(3R,5S,8S)-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1⁽²³⁾,17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonate

There total 1 articles about diethyl [1-({[(3R,5S,8S)-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1⁽²³⁾,17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl [(1S,2R)-1-amino-2-vinylcyclopropyl]phosphonate + (3R,5S,8S)-8-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1(23),17,19,21,24-pentaene-5-carboxylic acid (1021435-07-3) → diethyl [1-({[(3R,5S,8S)-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1(23),17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonate (1021488-44-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; HATU; dmap; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

diethyl [1-({[(3R,5S,8S)-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1(23),17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonate (1021488-44-7) → [1-({[(3R,5S,8S)-8-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1(23)-17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonic acid (1021488-45-8)

Guidance literature:

diethyl [1-({[(3R,5S,8S)-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1⁽²³⁾,17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonate; With 2,6-dimethylpyridine; trimethylsilyl iodide; In acetonitrile; at 0 - 20 ℃; for 21h;

With methanol; triethylamine; In acetonitrile;

upstream raw materials:

(3R,5S,8S)-8-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1⁽²³⁾,17,19,21,24-pentaene-5-carboxylic acid

Downstream raw materials:

[1-({[(3R,5S,8S)-8-cyclohexyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,23-triazatetracyclo[15.6.2.1~3,6~.0~20,24~]hexacosa-1⁽²³⁾-17,19,21,24-pentaen-5-yl]carbonyl}amino)-2-vinylcyclopropyl]phosphonic acid

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