Technology Process of 4-naphthalen-2-yl-benzoic acid 2,4-bis-octadecyloxybenzyl ester
There total 3 articles about 4-naphthalen-2-yl-benzoic acid 2,4-bis-octadecyloxybenzyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-iodobenzoic acid 2,4-bis-octadecyloxybenzyl ester;
With
tris-(o-tolyl)phosphine;
palladium diacetate;
In
N,N-dimethyl-formamide;
for 0.166667h;
naphthalene-2-boronic acid;
With
potassium dihydrogenphosphate;
In
cyclohexane; N,N-dimethyl-formamide;
at 80 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 100 °C / Inert atmosphere
1.2: 1 h / Cooling with ice
2.1: diisopropyl-carbodiimide; dmap / dichloromethane / 2 h / 20 °C
3.1: palladium diacetate; tris-(o-tolyl)phosphine; potassium phosphate / cyclohexane; N,N-dimethyl-formamide / 20 h / 80 °C
With
dmap; potassium phosphate; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine; diisopropyl-carbodiimide;
In
dichloromethane; cyclohexane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 100 °C / Inert atmosphere
1.2: 1 h / Cooling with ice
2.1: diisopropyl-carbodiimide; dmap / dichloromethane / 2 h / 20 °C
3.1: palladium diacetate; tris-(o-tolyl)phosphine; potassium phosphate / cyclohexane; N,N-dimethyl-formamide / 20 h / 80 °C
With
dmap; potassium phosphate; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine; diisopropyl-carbodiimide;
In
dichloromethane; cyclohexane; N,N-dimethyl-formamide;
