C₂₉H₂₇NO₄

Base Information

• Chemical Name: C₂₉H₂₇NO₄
• CAS No.: 1454786-27-6
• Molecular Formula: C₂₉H₂₇NO₄
• Molecular Weight: 453.538
• Mol file: 1454786-27-6.mol

Synonyms:C₂₉H₂₇NO₄

Chemical Property of C₂₉H₂₇NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₂₇NO₄

There total 2 articles about C₂₉H₂₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C32H31NO4 (1454786-14-1) → C29H27NO4 (1454786-27-6)

Guidance literature:

With (triphenylphosphine)gold(I) chloride; water; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; In dichloromethane; at 80 ℃; for 1h; diastereoselective reaction; Sealed tube;

DOI:10.1021/jo401390k

Reference yield:

C32H33NO5 (1454786-13-0) → C29H27NO4 (1454786-27-6)

Guidance literature:

Multi-step reaction with 2 steps

1: acetyl chloride; sodium hydroxide; tetra-(n-butyl)ammonium iodide / water; dichloromethane / 24 h / 20 °C

2: (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; water / dichloromethane / 1 h / 80 °C / Sealed tube

With (triphenylphosphine)gold(I) chloride; water; silver trifluoromethanesulfonate; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; acetyl chloride; sodium hydroxide; In dichloromethane; water;

DOI:10.1021/jo401390k

upstream raw materials:

C₃₂H₃₃NO₅

C₃₂H₃₁NO₄