(2R,3R) 1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-2-benzylaminosulfinyl-3-phenoxy-acetamido-4-oxo-azetidine

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Chemical Name:(2R,3R) 1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-2-benzylaminosulfinyl-3-phenoxy-acetamido-4-oxo-azetidine
CAS No.:153785-13-8
Molecular Formula:C₂₄H₂₇N₃O₆S
Molecular Weight:485.561
Hs Code.:

Synonyms:(2R,3R) 1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-2-benzylaminosulfinyl-3-phenoxy-acetamido-4-oxo-azetidine

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Chemical Property of (2R,3R) 1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-2-benzylaminosulfinyl-3-phenoxy-acetamido-4-oxo-azetidine

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Technology Process of (2R,3R) 1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-2-benzylaminosulfinyl-3-phenoxy-acetamido-4-oxo-azetidine

There total 2 articles about (2R,3R) 1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-2-benzylaminosulfinyl-3-phenoxy-acetamido-4-oxo-azetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.4%

: 153785-01-4
(R)-2-[(2R,3R)-2-Chlorosulfinyl-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-1-yl]-3-methyl-but-3-enoic acid methyl ester

: 100-46-9
benzylamine

: 153785-13-8
(2R,3R) 1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-2-benzylaminosulfinyl-3-phenoxy-acetamido-4-oxo-azetidine

Guidance literature:: In toluene; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80182-4

Reference yield:

: 10209-03-7
methyl 6β-phenoxyacetamidopenicillanate-1β-sulfoxide

: 153785-13-8
(2R,3R) 1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-2-benzylaminosulfinyl-3-phenoxy-acetamido-4-oxo-azetidine

Guidance literature:: Multi-step reaction with 2 steps

1: N-chlorosuccinimide, calcium oxide / toluene / 1.5 h / Heating

2: 74.4 percent / toluene / 2 h / Ambient temperature

With N-chloro-succinimide; calcium oxide; In toluene;
DOI:10.1016/S0040-4020(01)80182-4