methyl 2,6-di-O-benzyl-3-deoxy-3-C-(triethylammoniumsulfonatomethyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,6-di-O-benzyl-3-deoxy-3-C-(triethylammoniumsulfonatomethyl)-α-D-glucopyranoside
CAS No.:1161723-13-2
Molecular Formula:C₆H₁₅N*C₂₂H₂₈O₈S
Molecular Weight:553.717
Hs Code.:

Synonyms:methyl 2,6-di-O-benzyl-3-deoxy-3-C-(triethylammoniumsulfonatomethyl)-α-D-glucopyranoside

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Chemical Property of methyl 2,6-di-O-benzyl-3-deoxy-3-C-(triethylammoniumsulfonatomethyl)-α-D-glucopyranoside

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Technology Process of methyl 2,6-di-O-benzyl-3-deoxy-3-C-(triethylammoniumsulfonatomethyl)-α-D-glucopyranoside

There total 3 articles about methyl 2,6-di-O-benzyl-3-deoxy-3-C-(triethylammoniumsulfonatomethyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1161723-08-5
C₆H₁₅N*C₂₂H₂₆O₈S

: 121-44-8
triethylamine

: 1161723-13-2
methyl 2,6-di-O-benzyl-3-deoxy-3-C-(triethylammoniumsulfonatomethyl)-α-D-glucopyranoside

Guidance literature:: C₆H₁₅N*C₂₂H₂₆O₈S; With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 4h;

With water; sodium hydrogencarbonate; In dichloromethane;

triethylamine; With silica gel; In methanol; dichloromethane; regioselective reaction;
DOI:10.1021/ol900952d

Reference yield: 74.0%

: methyl 2,6-di-O-benzyl-3-deoxy-3-C-methylene-α-D-ribohexopyranoside

: 1161723-13-2
methyl 2,6-di-O-benzyl-3-deoxy-3-C-(triethylammoniumsulfonatomethyl)-α-D-glucopyranoside

Guidance literature:: With tert-Butyl peroxybenzoate; ethanol; water; sodium hydrogensulfite; for 4h; Reflux;
DOI:10.1016/j.carres.2011.06.021

Reference yield: 47.0%

: 1161723-09-6
C₂₂H₂₄O₅

: 1161723-13-2
methyl 2,6-di-O-benzyl-3-deoxy-3-C-(triethylammoniumsulfonatomethyl)-α-D-glucopyranoside

Guidance literature:: C₂₂H₂₄O₅; With tert-Butyl peroxybenzoate; ethanol; water; sodium hydrogensulfite; for 4h; Reflux;

With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1016/j.carres.2011.06.021