2,3,5,6-tetrafluoro-4-trifluoromethylphenylsulfenyl chloride

Base Information

• Chemical Name: 2,3,5,6-tetrafluoro-4-trifluoromethylphenylsulfenyl chloride
• CAS No.: 127538-39-0
• Molecular Formula: C₇ClF₇S
• Molecular Weight: 284.585
• Mol file: 127538-39-0.mol

Synonyms:2,3,5,6-tetrafluoro-4-trifluoromethylphenylsulfenyl chloride

Chemical Property of 2,3,5,6-tetrafluoro-4-trifluoromethylphenylsulfenyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,5,6-tetrafluoro-4-trifluoromethylphenylsulfenyl chloride

There total 1 articles about 2,3,5,6-tetrafluoro-4-trifluoromethylphenylsulfenyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-trifluoromethyl-2,3,5,6-tetrafluorothiophenol (651-84-3) → 2,3,5,6-tetrafluoro-4-trifluoromethylphenylsulfenyl chloride (127538-39-0)

Guidance literature:

With chlorine; In tetrachloromethane; at 20 ℃;

DOI:10.1002/ejic.200390016

Reference yield: 90.0%

2,3,5,6-tetrafluoro-4-trifluoromethylphenylsulfenyl chloride (127538-39-0) + potassium 1,2,3,4,5-pentakis(methoxycarbonyl)cyclopentadienide (16691-64-8) → 5-(2,3,5,6-Tetrafluoro-4-trifluoromethyl-phenylsulfanyl)-cyclopenta-1,3-diene-1,2,3,4,5-pentacarboxylic acid pentamethyl ester (122180-54-5)

Guidance literature:

In benzene; for 4h; Ambient temperature;

Reference yield: 84.0%

N,N'-bis(trimethylsilyl)sulfurdiimide (503027-47-2,503027-48-3,155139-78-9,18156-25-7) + 2,3,5,6-tetrafluoro-4-trifluoromethylphenylsulfenyl chloride (127538-39-0) → 1-[2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl]-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene (530102-88-6)

Guidance literature:

In dichloromethane; at 20 ℃; for 16h;

DOI:10.1002/ejic.200390016

upstream raw materials:

4-trifluoromethyl-2,3,5,6-tetrafluorothiophenol

Downstream raw materials:

5-Methyl-1-(2,3,5,6-tetrafluoro-4-trifluoromethyl-phenylsulfanyl)-cyclopenta-2,4-diene-1,2,3,4-tetracarboxylic acid tetramethyl ester

5-Methyl-3-(2,3,5,6-tetrafluoro-4-trifluoromethyl-phenylsulfanyl)-cyclopenta-1,4-diene-1,2,3,4-tetracarboxylic acid tetramethyl ester

5-(2,3,5,6-Tetrafluoro-4-trifluoromethyl-phenylsulfanyl)-cyclopenta-1,3-diene-1,2,3,4,5-pentacarboxylic acid pentamethyl ester

5-methoxy-3-methyl-1-phenyl-4-(2,3,5,6-tetrafluoro-4-trifluoromethyl-phenylsulfanyl)-1H-pyrazole