(Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl fluoride

Base Information

Chemical Name:(Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl fluoride
CAS No.:690663-24-2
Molecular Formula:C₁₀H₆F₇NO
Molecular Weight:289.153
Hs Code.:

Synonyms:(Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl fluoride

Suppliers and Price of (Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl fluoride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl fluoride

Chemical Property:

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Technology Process of (Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl fluoride

There total 3 articles about (Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 690663-23-1
(Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl bromide

: 690663-24-2
(Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl fluoride

Guidance literature:: With potassium fluoride; In dimethyl sulfoxide; at 100 ℃; for 22h;
DOI:10.1021/jo030299e

Reference yield:

: 785-56-8
3,5-bis(trifluoromethyl)phenyl carboxylic acid chloride

: 690663-24-2
(Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl fluoride

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / phosphorus pentabromide / 3 h / 80 °C

2: 97 percent / potassium fluoride / dimethylsulfoxide / 22 h / 100 °C

With potassium fluoride; phosphorus pentabromide; In dimethyl sulfoxide;
DOI:10.1021/jo030299e

Reference yield:

: 690663-30-0
methyl 3,5-bistrifluoromethylbenzohydroxamate

: 690663-24-2
(Z)-O-methyl-3,5-bistrifluoromethylbenzohydroximoyl fluoride

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / phosphorus pentabromide / 3 h / 80 °C

2: 97 percent / potassium fluoride / dimethylsulfoxide / 22 h / 100 °C

With potassium fluoride; phosphorus pentabromide; In dimethyl sulfoxide;
DOI:10.1021/jo030299e