Tetracyclo(5.2.1.02,6.03,5)decane, (1alpha,2alpha,3beta,5beta,6alpha,7alpha)-

Base Information

• Chemical Name: Tetracyclo(5.2.1.02,6.03,5)decane, (1alpha,2alpha,3beta,5beta,6alpha,7alpha)-
• CAS No.: 53862-36-5
• Molecular Formula: C₁₀H₁₄
• Molecular Weight: 134.221
• DSSTox Substance ID: DTXSID80968634
• Mol file: 53862-36-5.mol

Synonyms:53862-36-5;Tetracyclo(5.2.1.02,6.03,5)decane, (1alpha,2alpha,3beta,5beta,6alpha,7alpha)-;DTXSID80968634;Tetracyclo[5.2.1.0~2,6~.0~3,5~]decane;Tetracyclo[5.2.1.02,6.03,5]decane,(1.alpha.,2.alpha.,3.beta.,5.beta.,6.alpha.,7.alpha.)-

Chemical Property of Tetracyclo(5.2.1.02,6.03,5)decane, (1alpha,2alpha,3beta,5beta,6alpha,7alpha)-

Chemical Property:

• Vapor Pressure: 0.982mmHg at 25°C
• Boiling Point: 184.9°Cat760mmHg
• Flash Point: 44.7°C
• Density: 1.114g/cm³
• XLogP3: 3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 134.109550447
• Heavy Atom Count: 10
• Complexity: 176

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC2CC1C3C2C4C3C4

Technology Process of Tetracyclo(5.2.1.02,6.03,5)decane, (1alpha,2alpha,3beta,5beta,6alpha,7alpha)-

There total 4 articles about Tetracyclo(5.2.1.02,6.03,5)decane, (1alpha,2alpha,3beta,5beta,6alpha,7alpha)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

syn-4,5-diazatetracyclo<6.2.1.13,6.02,7>dodec-4-ene (74987-36-3) → endo,anti-tetracyclo<5.2.1.02,6.03,5>decane (53862-36-5)

Guidance literature:

In acetone; for 2h; Irradiation;

DOI:10.1021/jo01312a020

Reference yield:

tricyclo<5.2.1.02,6>deca-2,5,-diene (6675-72-5) → endo,anti-tetracyclo<5.2.1.02,6.03,5>decane (53862-36-5)

Guidance literature:

Multi-step reaction with 4 steps

1: 88 percent / ethyl acetate / -35 °C

2: 15.6 percent / hydrazine (97percent), hydrogen peroxide (30percent) / ethanol / 1) 0 deg C, 30 min, 2) room temp.

4: 59 percent / acetone / 2 h / Irradiation

With dihydrogen peroxide; hydrazine hydrate; In ethanol; ethyl acetate; acetone;

DOI:10.1021/jo01312a020

Reference yield:

C13H15N3O2 (73321-35-4) → endo,anti-tetracyclo<5.2.1.02,6.03,5>decane (53862-36-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 15.6 percent / hydrazine (97percent), hydrogen peroxide (30percent) / ethanol / 1) 0 deg C, 30 min, 2) room temp.

3: 59 percent / acetone / 2 h / Irradiation

With dihydrogen peroxide; hydrazine hydrate; In ethanol; acetone;

DOI:10.1021/jo01312a020

upstream raw materials:

syn-4,5-diazatetracyclo<6.2.1.1^3,6.0^2,7>dodec-4-ene

tricyclo<5.2.1.0^2,6>deca-2,5,-diene

C₁₃H₁₇N₃O₂

C₁₃H₁₅N₃O₂