2,7-bis(4-nitrophenoxy)-9-fluorenone

Base Information

Chemical Name:2,7-bis(4-nitrophenoxy)-9-fluorenone
CAS No.:1332524-31-8
Molecular Formula:C₂₅H₁₄N₂O₇
Molecular Weight:454.395
Hs Code.:

Synonyms:2,7-bis(4-nitrophenoxy)-9-fluorenone

Suppliers and Price of 2,7-bis(4-nitrophenoxy)-9-fluorenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,7-bis(4-nitrophenoxy)-9-fluorenone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,7-bis(4-nitrophenoxy)-9-fluorenone

There total 1 articles about 2,7-bis(4-nitrophenoxy)-9-fluorenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.2%

: 42523-29-5
2,7-dihydroxy-9H-fluoren-9-one

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1332524-31-8
2,7-bis(4-nitrophenoxy)-9-fluorenone

Guidance literature:: With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 90 ℃; for 3h; Inert atmosphere;

Reference yield: 100.0%

: 1332524-31-8
2,7-bis(4-nitrophenoxy)-9-fluorenone

: 1332524-32-9
2,7-bis(4-nitrophenoxy)-9-hydroxyfluorene

Guidance literature:: 2,7-bis(4-nitrophenoxy)-9-fluorenone; With aluminum (III) chloride; sodium tetrahydroborate; In tetrahydrofuran; Inert atmosphere;

With water; In tetrahydrofuran; Cooling with ice;

Reference yield:

: 1332524-31-8
2,7-bis(4-nitrophenoxy)-9-fluorenone

: 1332524-34-1
2,7-bis(4-aminophenoxy)fluorene

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride; sodium tetrahydroborate / tetrahydrofuran / Inert atmosphere

1.2: Cooling with ice

2.1: dmap / dichloromethane / 20 °C / Cooling with ice; Inert atmosphere

3.1: hydrogen / 10-wt percent palladium-activated carbon ethylenediamine complex / tetrahydrofuran / 48 h / 20 °C

With dmap; aluminum (III) chloride; sodium tetrahydroborate; hydrogen; 10-wt percent palladium-activated carbon ethylenediamine complex; In tetrahydrofuran; dichloromethane;