1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl 3-methyl-3-butenyl peroxide

Base Information

Chemical Name:1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl 3-methyl-3-butenyl peroxide
CAS No.:525552-15-2
Molecular Formula:C₂₂H₄₄O₅Si
Molecular Weight:416.674
Hs Code.:

Synonyms:1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl 3-methyl-3-butenyl peroxide

Suppliers and Price of 1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl 3-methyl-3-butenyl peroxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl 3-methyl-3-butenyl peroxide

Chemical Property:

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Technology Process of 1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl 3-methyl-3-butenyl peroxide

There total 4 articles about 1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl 3-methyl-3-butenyl peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 53750-52-0
4-iodo-2-methyl-but-1-ene

: 525552-13-0
1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl hydroperoxide

: 525552-15-2
1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl 3-methyl-3-butenyl peroxide

Guidance literature:: With silver(l) oxide; In dichloromethane; at 20 ℃; for 17h;
DOI:10.1016/S0040-4020(02)01556-9

Reference yield:

: 763-32-6
2-methyl-1-buten-4-ol

: 525552-15-2
1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl 3-methyl-3-butenyl peroxide

Guidance literature:: Multi-step reaction with 3 steps

1: 26 percent / (1-morpholinocarbamoyl-4,4-Me₂-1,3-pentanedionato)2Co(II) / CH₂Cl₂ / 3 h / 20 °C

2: 63 percent / O₃ / CH₂Cl₂ / -70 °C

3: 17 percent / Ag₂O / CH₂Cl₂ / 17 h / 20 °C

With (1-morpholinocarbamoyl-4,4-Me₂-1,3-pentanedionato)2Co(II); ozone; silver(l) oxide; In dichloromethane;
DOI:10.1016/S0040-4020(02)01556-9

Reference yield:

: 617-86-7
triethylsilane

: 525552-15-2
1-[[3-methyl-3-(triethylsilyl)dioxy]butoxy]cyclohexyl 3-methyl-3-butenyl peroxide

Guidance literature:: Multi-step reaction with 3 steps

1: 26 percent / (1-morpholinocarbamoyl-4,4-Me₂-1,3-pentanedionato)2Co(II) / CH₂Cl₂ / 3 h / 20 °C

2: 63 percent / O₃ / CH₂Cl₂ / -70 °C

3: 17 percent / Ag₂O / CH₂Cl₂ / 17 h / 20 °C

With (1-morpholinocarbamoyl-4,4-Me₂-1,3-pentanedionato)2Co(II); ozone; silver(l) oxide; In dichloromethane;
DOI:10.1016/S0040-4020(02)01556-9