3',5'-diaminoacetophenone

Base Information

• Chemical Name: 3',5'-diaminoacetophenone
• CAS No.: 33786-92-4
• Molecular Formula: C8H10N2O
• Molecular Weight: 150.18
• Hs Code.: 2922399090
• Mol file: 33786-92-4.mol

Synonyms:Acetophenone,3',5'-diamino- (8CI);3',5'-Diaminoacetophenone;

Chemical Property of 3',5'-diaminoacetophenone

Chemical Property:

• Boiling Point: 392.774 °C at 760 mmHg
• Flash Point: 191.343 °C
• PSA: 69.11000
• Density: 1.196 g/cm³
• LogP: 2.21600

Purity/Quality:

98%Min ^*data from raw suppliers

3',5'-DIAMINOACETOPHENONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3',5'-diaminoacetophenone

There total 1 articles about 3',5'-diaminoacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3,5-dinitrophenyl)ethanone (14401-75-3) → 3,5-diaminoacetophenone (33786-92-4)

Guidance literature:

With hydrogenchloride; tin;

Reference yield: 89.0%

3,5-diaminoacetophenone (33786-92-4) + (E)-3,4-dimethoxycinnamic chloride (39856-08-1,141236-46-6) → 3,5-bis(3,4-dimethoxycinnamoylamino)acetophenone

Guidance literature:

3,5-diaminoacetophenone; (E)-3,4-dimethoxycinnamic chloride; With pyridine; In dichloromethane; at 20 ℃;

With water; In dichloromethane;

In chloroform; for 4h;

DOI:10.1021/jm1010594

Reference yield:

3,5-diaminoacetophenone (33786-92-4) → 5-ethylbenzene-1,3-diamine (408309-32-0)

Guidance literature:

With potassium hydroxide; hydrazine hydrate; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol;

DOI:10.1007/BF00897796

upstream raw materials:

1-(3,5-dinitrophenyl)ethanone

Downstream raw materials:

5-ethylbenzene-1,3-diamine

1-(3,5-bis-acetylamino-phenyl)-ethanone

3-ethyl-5-amino-phenol