Technology Process of C51H72N10O15S2
There total 1 articles about C51H72N10O15S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; water;
at 20 ℃;
DOI:10.1021/jm301058f
- Guidance literature:
-
With
benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; HATU;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1021/jm301058f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine; HATU; benzotriazol-1-ol / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
2.1: methyl-phenyl-thioether; ethane-1,2-dithiol; phenol; trimethylsilyl bromide / 2 h / 0 - 20 °C / Inert atmosphere
3.1: 1-hydroxy-pyrrolidine-2,5-dione; di-isopropyl azodicarboxylate / dichloromethane / 2 h / 20 °C / Inert atmosphere
3.2: 28 h / 0 - 20 °C / pH 7.3
With
1-hydroxy-pyrrolidine-2,5-dione; trimethylsilyl bromide; methyl-phenyl-thioether; di-isopropyl azodicarboxylate; benzotriazol-1-ol; ethane-1,2-dithiol; N-ethyl-N,N-diisopropylamine; HATU; phenol;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301058f