9-Methoxy-16,18-diphenyl-2,11-dithia<3>metacyclo<3>(2,6)pyranophan-17-on-2,2,11,11-tetroxid

Base Information

Chemical Name:9-Methoxy-16,18-diphenyl-2,11-dithia<3>metacyclo<3>(2,6)pyranophan-17-on-2,2,11,11-tetroxid
CAS No.:124991-99-7
Molecular Formula:C₂₈H₂₄O₇S₂
Molecular Weight:536.626
Hs Code.:

Synonyms:9-Methoxy-16,18-diphenyl-2,11-dithia<3>metacyclo<3>(2,6)pyranophan-17-on-2,2,11,11-tetroxid

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Chemical Property of 9-Methoxy-16,18-diphenyl-2,11-dithia<3>metacyclo<3>(2,6)pyranophan-17-on-2,2,11,11-tetroxid

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Technology Process of 9-Methoxy-16,18-diphenyl-2,11-dithia<3>metacyclo<3>(2,6)pyranophan-17-on-2,2,11,11-tetroxid

There total 3 articles about 9-Methoxy-16,18-diphenyl-2,11-dithia<3>metacyclo<3>(2,6)pyranophan-17-on-2,2,11,11-tetroxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 124945-43-3
9-Methoxy-16,18-diphenyl-2,11-dithia<3>metacyclo<3>(2,6)pyranophan-17-on

: 124991-99-7
9-Methoxy-16,18-diphenyl-2,11-dithia<3>metacyclo<3>(2,6)pyranophan-17-on-2,2,11,11-tetroxid

Guidance literature:: With dihydrogen peroxide; In acetic acid; for 3h; Heating;

Reference yield:

: 33731-54-3
2,6-dimethyl-3,5-diphenyl-4H-pyran-4-one

: 124991-99-7
9-Methoxy-16,18-diphenyl-2,11-dithia<3>metacyclo<3>(2,6)pyranophan-17-on-2,2,11,11-tetroxid

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl₄ / 48 h / Heating

2: 21 percent / KOH / CHCl₃; ethanol / 72 h / Heating

3: 80 percent / 30percent aq. H₂O₂ / acetic acid / 3 h / Heating

With potassium hydroxide; N-Bromosuccinimide; dihydrogen peroxide; dibenzoyl peroxide; In tetrachloromethane; ethanol; chloroform; acetic acid;

Reference yield:

: 124945-37-5
2,6-Bis(brommethyl)-3,5-diphenyl-4-pyranon

: 124991-99-7
9-Methoxy-16,18-diphenyl-2,11-dithia<3>metacyclo<3>(2,6)pyranophan-17-on-2,2,11,11-tetroxid

Guidance literature:: Multi-step reaction with 2 steps

1: 21 percent / KOH / CHCl₃; ethanol / 72 h / Heating

2: 80 percent / 30percent aq. H₂O₂ / acetic acid / 3 h / Heating

With potassium hydroxide; dihydrogen peroxide; In ethanol; chloroform; acetic acid;