1-[2-(4-Methoxyphenyl)-1-ethynyl]-4-propylbenzene

Base Information

• Chemical Name: 1-[2-(4-Methoxyphenyl)-1-ethynyl]-4-propylbenzene
• CAS No.: 39969-26-1
• Molecular Formula: C18H18O
• Molecular Weight: 250.34
• Hs Code.: 2909309090
• Mol file: 39969-26-1.mol

Synonyms:Benzene,1-[(4-methoxyphenyl)ethynyl]-4-propyl- (9CI);PTP 3O1;p-[(p-Propylphenyl)ethynyl]anisole;Benzene,1-[2-(4-methoxyphenyl)ethynyl]-4-propyl-;

Chemical Property of 1-[2-(4-Methoxyphenyl)-1-ethynyl]-4-propylbenzene

Chemical Property:

• Vapor Pressure: 1.45E-05mmHg at 25°C
• Melting Point: 61ºC
• Refractive Index: 1.58
• Boiling Point: 377.6ºC at 760 mmHg
• Flash Point: 180ºC
• PSA: 9.23000
• Density: 1.05g/cm³
• LogP: 4.04750
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

1-Methoxy-4-((4-propylphenyl)ethynyl)benzene 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[2-(4-Methoxyphenyl)-1-ethynyl]-4-propylbenzene

There total 1 articles about 1-[2-(4-Methoxyphenyl)-1-ethynyl]-4-propylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-methoxy-4-((4-propylphenyl)ethynyl)benzene (39969-26-1)

Guidance literature:

entspr. 1,1-Diphenyl-aethylen, t-BuOK, 200grad;

Reference yield: 93.0%

1-methoxy-4-((4-propylphenyl)ethynyl)benzene (39969-26-1) → 1-methoxy-4-[(1Z)-2-(4-propylphenyl)ethenyl]benzene

Guidance literature:

With triethanolamine; sodium acetate; palladium diacetate; In ethanol; acetonitrile; at 140 ℃; for 32h;

Reference yield: 74.0%

1-methoxy-4-((4-propylphenyl)ethynyl)benzene (39969-26-1) + 1,2-diamino-benzene (95-54-5) → C24H22N2O

Guidance literature:

With dimethyl sulfoxide; at 140 ℃; for 10h; Sealed tube;

DOI:10.1007/s11164-019-03918-w

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