5-{4-[5-(5-Diethoxymethyl-furan-2-yl)-pentyloxy]-3,5-dimethyl-phenyl}-2-methyl-2H-tetrazole

Base Information

Chemical Name:5-{4-[5-(5-Diethoxymethyl-furan-2-yl)-pentyloxy]-3,5-dimethyl-phenyl}-2-methyl-2H-tetrazole
CAS No.:1026603-32-6
Molecular Formula:C₂₄H₃₄N₄O₄
Molecular Weight:442.558
Hs Code.:

Synonyms:5-{4-[5-(5-Diethoxymethyl-furan-2-yl)-pentyloxy]-3,5-dimethyl-phenyl}-2-methyl-2H-tetrazole

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Chemical Property of 5-{4-[5-(5-Diethoxymethyl-furan-2-yl)-pentyloxy]-3,5-dimethyl-phenyl}-2-methyl-2H-tetrazole

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Technology Process of 5-{4-[5-(5-Diethoxymethyl-furan-2-yl)-pentyloxy]-3,5-dimethyl-phenyl}-2-methyl-2H-tetrazole

There total 3 articles about 5-{4-[5-(5-Diethoxymethyl-furan-2-yl)-pentyloxy]-3,5-dimethyl-phenyl}-2-methyl-2H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 152665-33-3
2-methyl-5-(3,5-dimethyl-4-hydroxyphenyl)-2H-tetrazole

: 159727-78-3
2-(5-chloropentyl)-5-(diethoxymethyl)furan

: 1026603-32-6
5-{4-[5-(5-Diethoxymethyl-furan-2-yl)-pentyloxy]-3,5-dimethyl-phenyl}-2-methyl-2H-tetrazole

Guidance literature:: With potassium hydroxide; potassium iodide; In acetonitrile; for 14h; Heating;
DOI:10.1021/jm00050a014

Reference yield:

: 13529-27-6
2-(diethoxymethyl)furan

: 1026603-32-6
5-{4-[5-(5-Diethoxymethyl-furan-2-yl)-pentyloxy]-3,5-dimethyl-phenyl}-2-methyl-2H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuLi / 1.) THF, pentane, -70 deg C, 15 min, 2.) THF, pentane, HMPA, RT, 12 h

2: 60 percent / KOH, KI / acetonitrile / 14 h / Heating

With potassium hydroxide; tert.-butyl lithium; potassium iodide; In acetonitrile;
DOI:10.1021/jm00050a014

Reference yield:

: 54512-75-3
1-bromo-5-chloropentane

: 1026603-32-6
5-{4-[5-(5-Diethoxymethyl-furan-2-yl)-pentyloxy]-3,5-dimethyl-phenyl}-2-methyl-2H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuLi / 1.) THF, pentane, -70 deg C, 15 min, 2.) THF, pentane, HMPA, RT, 12 h

2: 60 percent / KOH, KI / acetonitrile / 14 h / Heating

With potassium hydroxide; tert.-butyl lithium; potassium iodide; In acetonitrile;
DOI:10.1021/jm00050a014