N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide

Base Information

Chemical Name:N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide
CAS No.:160978-33-6
Molecular Formula:C₂₀H₂₉N₃O₅S
Molecular Weight:423.533
Hs Code.:

N<sup>α</sup>-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide

Synonyms:N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide

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Chemical Property of N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide

Chemical Property:

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Technology Process of N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide

There total 3 articles about N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 100-46-9
benzylamine

: 204074-79-3
N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine

: 160978-33-6
N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 5h;
DOI:10.1016/S0040-4020(99)00322-1

Reference yield:

: 24935-97-5
allyl N-hydroxymethyl carbamate

: 160978-33-6
N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / trifluoroacetic acid / CH₂Cl₂ / 0.17 h / 20 °C

2: 2.13 g / triethylamine / H₂O; dioxane / 3 h / 20 °C

3: 50 percent / HOBt; dicyclohexylcarbodiimide / dimethylformamide / 5 h / 0 - 20 °C

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; 1: Condensation / 2: Condensation / 3: Condensation;
DOI:10.1016/S0040-4020(99)00322-1

Reference yield:

: S-allyloxycarbonylaminomethyl L-cysteine hydrochloride

: 160978-33-6
N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2.13 g / triethylamine / H₂O; dioxane / 3 h / 20 °C

2: 50 percent / HOBt; dicyclohexylcarbodiimide / dimethylformamide / 5 h / 0 - 20 °C

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; water; N,N-dimethyl-formamide; 1: Condensation / 2: Condensation;
DOI:10.1016/S0040-4020(99)00322-1