C₄₁H₄₂N₂O₇Si

Base Information

Chemical Name:C₄₁H₄₂N₂O₇Si
CAS No.:1092804-54-0
Molecular Formula:C₄₁H₄₂N₂O₇Si
Molecular Weight:702.879
Hs Code.:

C<sub>41</sub>H<sub>42</sub>N<sub>2</sub>O<sub>7</sub>Si

Synonyms:C₄₁H₄₂N₂O₇Si

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Chemical Property of C₄₁H₄₂N₂O₇Si

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Technology Process of C₄₁H₄₂N₂O₇Si

There total 12 articles about C₄₁H₄₂N₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₄₂O₇Si

: 66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6
uracil

: 1092804-54-0
C₄₁H₄₂N₂O₇Si

Guidance literature:: With N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate; In acetonitrile; for 2h; Cooling with ice; Reflux;

Reference yield:

: 2595-05-3
Diacetone D-glucose

: 1092804-54-0
C₄₁H₄₂N₂O₇Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1.17 h / Cooling with ice

2.1: water; acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane; water / 1.67 h

4.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

5.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

7.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

7.2: 16.33 h / -78 - 20 °C

8.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

8.2: 4 h / 50 °C

9.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

9.2: 0.5 h

10.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C

10.2: 2 h / -78 °C

11.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C

12.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C

13.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

14.1: sulfuric acid / 0.25 h / 20 °C

15.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 2 h / Cooling with ice; Reflux

With sodium periodate; n-butyllithium; N,O-bis-(trimethylsilyl)-acetamide; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; water; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil; 15.1: Vorbrugen reaction;

Reference yield:

: 956485-06-6
3-O-(2-naphthylmethyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 1092804-54-0
C₄₁H₄₂N₂O₇Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: water; acetic acid / 16 h / 20 °C

2.1: sodium periodate / 1,4-dioxane; water / 1.67 h

3.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

4.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

6.2: 16.33 h / -78 - 20 °C

7.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

7.2: 4 h / 50 °C

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

8.2: 0.5 h

9.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C

9.2: 2 h / -78 °C

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C

11.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C

12.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

13.1: sulfuric acid / 0.25 h / 20 °C

14.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 2 h / Cooling with ice; Reflux

With sodium periodate; n-butyllithium; N,O-bis-(trimethylsilyl)-acetamide; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; water; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil; 14.1: Vorbrugen reaction;