2-methoxy-3-(3'-methyl-2'-butenyl)-4-<(dimethylamino)methyl>-6-methylphenol

Base Information

Chemical Name:2-methoxy-3-(3'-methyl-2'-butenyl)-4-<(dimethylamino)methyl>-6-methylphenol
CAS No.:127785-63-1
Molecular Formula:C₁₆H₂₅NO₂
Molecular Weight:263.38
Hs Code.:

Synonyms:2-methoxy-3-(3'-methyl-2'-butenyl)-4-<(dimethylamino)methyl>-6-methylphenol

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Chemical Property of 2-methoxy-3-(3'-methyl-2'-butenyl)-4-<(dimethylamino)methyl>-6-methylphenol

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Technology Process of 2-methoxy-3-(3'-methyl-2'-butenyl)-4-<(dimethylamino)methyl>-6-methylphenol

There total 6 articles about 2-methoxy-3-(3'-methyl-2'-butenyl)-4-<(dimethylamino)methyl>-6-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [3-Methoxy-5-methyl-2-((E)-3-methyl-3-trimethylsilanyloxy-but-1-enyl)-4-trimethylsilanyloxy-benzyl]-dimethyl-amine

: 127785-63-1
2-methoxy-3-(3'-methyl-2'-butenyl)-4-<(dimethylamino)methyl>-6-methylphenol

Guidance literature:: With ammonia; lithium; In tetrahydrofuran; at -78 ℃; for 0.25h; Yield given;
DOI:10.1021/jo00054a012

Reference yield:

: 127757-19-1
3-(3'-hydroxy-3'-methylbutenyl)-2-methoxy-4-<(dimethylamino)methyl>-6-methylphenol

: 127785-63-1
2-methoxy-3-(3'-methyl-2'-butenyl)-4-<(dimethylamino)methyl>-6-methylphenol

Guidance literature:: With chloro-trimethyl-silane; lithium; 1,1,1,3,3,3-hexamethyl-disilazane; Yield given. Multistep reaction; 1.) THF, 0 deg C, 2.) liq. NH₃, THF;
DOI:10.1016/S0040-4039(00)88801-2

Reference yield:

: 104113-84-0
4-<(dimethylamino)methyl>-2-methoxy-6-methylphenol

: 127785-63-1
2-methoxy-3-(3'-methyl-2'-butenyl)-4-<(dimethylamino)methyl>-6-methylphenol

Guidance literature:: Multi-step reaction with 4 steps

1: 1) n-BuLi / 1a) THF, 0 deg C, 10 min, 1b) to r.t., 2 h, 2) 0 deg C, 3 h

2: 85percent H₃PO₄ / dioxane / 4 h

3: NEt₃ / tetrahydrofuran / 2 h / Ambient temperature

4: Li, NH₃ / tetrahydrofuran / 0.25 h / -78 °C

With n-butyllithium; phosphoric acid; ammonia; lithium; triethylamine; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jo00054a012