12-phenyl-10,11,12,12a,13,14,15,16-octahydro-benzo[c]benzo[4,5][1,4]oxazino[3,2-f]acridin-18-one

Base Information

Chemical Name:12-phenyl-10,11,12,12a,13,14,15,16-octahydro-benzo[c]benzo[4,5][1,4]oxazino[3,2-f]acridin-18-one
CAS No.:70194-71-7
Molecular Formula:C₃₀H₂₇NO₂
Molecular Weight:433.55
Hs Code.:

12-phenyl-10,11,12,12a,13,14,15,16-octahydro-benzo[<i>c</i>]benzo[4,5][1,4]oxazino[3,2-<i>f</i>]acridin-18-one

Synonyms:12-phenyl-10,11,12,12a,13,14,15,16-octahydro-benzo[c]benzo[4,5][1,4]oxazino[3,2-f]acridin-18-one

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Chemical Property of 12-phenyl-10,11,12,12a,13,14,15,16-octahydro-benzo[c]benzo[4,5][1,4]oxazino[3,2-f]acridin-18-one

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Technology Process of 12-phenyl-10,11,12,12a,13,14,15,16-octahydro-benzo[c]benzo[4,5][1,4]oxazino[3,2-f]acridin-18-one

There total 1 articles about 12-phenyl-10,11,12,12a,13,14,15,16-octahydro-benzo[c]benzo[4,5][1,4]oxazino[3,2-f]acridin-18-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65419-99-0
2-<(2-Cyclohexanoyl)phenylmethyl>-1-tetralone

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 70194-71-7
12-phenyl-10,11,12,12a,13,14,15,16-octahydro-benzo[c]benzo[4,5][1,4]oxazino[3,2-f]acridin-18-one

Guidance literature:: With toluene-4-sulfonic acid; In xylene; for 30h; Heating;
DOI:10.1007/BF00480368

Reference yield: 82.0%

: 70194-71-7
12-phenyl-10,11,12,12a,13,14,15,16-octahydro-benzo[c]benzo[4,5][1,4]oxazino[3,2-f]acridin-18-one

: 75065-48-4
2-(7-Phenyl-5,7,7a,8,9,10,11,11a-octahydro-6H-benzo[c]acridin-12-yl)-benzoic acid

Guidance literature:: With potassium borohydride; In 1,4-dioxane; water; for 2h;
DOI:10.1007/BF00552780

Reference yield:

: 70194-71-7
12-phenyl-10,11,12,12a,13,14,15,16-octahydro-benzo[c]benzo[4,5][1,4]oxazino[3,2-f]acridin-18-one

: 75065-50-8
2-((6aR,12aS)-7-Phenyl-5,6a,7,7a,8,9,10,11,11a,12a-decahydro-6H-benzo[c]acridin-12-yl)-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / KBH₄ / dioxane; H₂O / 2 h

2: KBH₄ / dimethylformamide / 1.5 h / Heating

With potassium borohydride; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1007/BF00552780