Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-carbamic acid methyl ester

Base Information

Chemical Name:Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-carbamic acid methyl ester
CAS No.:148679-74-7
Molecular Formula:C₁₈H₁₉NO₄S
Molecular Weight:345.419
Hs Code.:

Synonyms:Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-carbamic acid methyl ester

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Chemical Property of Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-carbamic acid methyl ester

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Technology Process of Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-carbamic acid methyl ester

There total 5 articles about Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-carbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 148679-74-7
Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: p-TsOH / benzene / Heating

2: NaBH₄ / methanol / 2 h / Ambient temperature

3: CH₂Cl₂ / 2 h / 0 °C

With sodium tetrahydroborate; toluene-4-sulfonic acid; In methanol; dichloromethane; benzene;
DOI:10.3987/COM-92-S14

Reference yield:

: 2014-75-7
2-(phenylthio)ethanamine

: 148679-74-7
Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: p-TsOH / benzene / Heating

2: NaBH₄ / methanol / 2 h / Ambient temperature

3: CH₂Cl₂ / 2 h / 0 °C

With sodium tetrahydroborate; toluene-4-sulfonic acid; In methanol; dichloromethane; benzene;
DOI:10.3987/COM-92-S14

Reference yield:

: 41010-04-2
4-nitro-2-(2-(phenylthio)ethyl)isoindoline-1,3-dione

: 148679-74-7
Benzo[1,3]dioxol-5-ylmethyl-(2-phenylsulfanyl-ethyl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NH₂NH₂*H₂O / ethanol / 1 h / Heating

2: p-TsOH / benzene / Heating

3: NaBH₄ / methanol / 2 h / Ambient temperature

4: CH₂Cl₂ / 2 h / 0 °C

With sodium tetrahydroborate; toluene-4-sulfonic acid; hydrazine hydrate; In methanol; ethanol; dichloromethane; benzene;
DOI:10.3987/COM-92-S14