butane-1,1,2-triyltribenzene

Base Information

• Chemical Name: butane-1,1,2-triyltribenzene
• CAS No.: 152076-78-3
• Molecular Formula: C₂₂H₂₂
• Molecular Weight: 286.417
• Mol file: 152076-78-3.mol

Synonyms:butane-1,1,2-triyltribenzene

Chemical Property of butane-1,1,2-triyltribenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of butane-1,1,2-triyltribenzene

There total 9 articles about butane-1,1,2-triyltribenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Diphenylmethane (101-81-5) + C21H21O4P → butane-1,1,2-triyltribenzene (152076-78-3)

Guidance literature:

Diphenylmethane; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 15 ℃; for 0.25h;

C₂₁H₂₁O₄P; In tetrahydrofuran; hexane; at -15 ℃; for 0.25h; enantioselective reaction;

DOI:10.1016/j.tet.2019.03.050

Reference yield: 79.0%

Diphenylmethane (101-81-5) + (+/-)-diethyl 1-phenylpropyl phosphate (34881-07-7) → 1,1-diphenylpropane (1530-03-6) + butane-1,1,2-triyltribenzene (152076-78-3)

Guidance literature:

Diphenylmethane; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 15 ℃; for 0.25h;

(+/-)-diethyl 1-phenylpropyl phosphate; In tetrahydrofuran; hexane; at -15 ℃; for 0.25h; enantioselective reaction;

DOI:10.1016/j.tet.2019.03.050

Reference yield:

but-1-ene-1,1,2-triyltribenzene (63019-13-6) → butane-1,1,2-triyltribenzene (152076-78-3)

Guidance literature:

With hydrogen; In ethanol; water; at 50 ℃; under 7500.75 Torr;

DOI:10.1002/anie.201912640

upstream raw materials:

1-Phenyl-1-propanol

Diphenylmethane

(+/-)-diethyl 1-phenylpropyl phosphate

1-phenyl-propan-1-one