C₂₅H₂₇N₃O₇

Base Information Edit

Chemical Name:C₂₅H₂₇N₃O₇
CAS No.:1300589-85-8
Molecular Formula:C₂₅H₂₇N₃O₇
Molecular Weight:481.505
Hs Code.:
Mol file:1300589-85-8.mol

C<sub>25</sub>H<sub>27</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₂₅H₂₇N₃O₇

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Chemical Property of C₂₅H₂₇N₃O₇ Edit

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Technology Process of C₂₅H₂₇N₃O₇

There total 11 articles about C₂₅H₂₇N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300589-82-5
C₂₅H₂₅N₅O₇

: 1300589-85-8
C₂₅H₂₇N₃O₇

Guidance literature:: With tributylphosphine; water; In tetrahydrofuran; at 20 ℃; for 3.5h;

Reference yield:

: 1300589-59-6
C₄₀H₄₆O₈Si

: 1300589-85-8
C₂₅H₂₇N₃O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1 h / 20 °C / Inert atmosphere; Reflux

2.1: methylamine / water; tetrahydrofuran / 0.5 h / 20 °C

3.1: dmap; trifluoromethane sulfonyl chloride / dichloromethane / 1 h / 20 °C / Inert atmosphere; Cooling with ice

4.1: sodium hydroxide; water / tetrahydrofuran / 1.5 h / 20 °C

5.1: pyridine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

6.1: sodium azide / N,N-dimethyl-formamide / 48 h / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12.5 h / Inert atmosphere

8.1: dipyridinium dichromate / N,N-dimethyl-formamide / 4.5 h / 20 °C / Inert atmosphere; Molecular sieve

8.2: 1 h

9.1: water; tributylphosphine / tetrahydrofuran / 3.5 h / 20 °C

With pyridine; dmap; dipyridinium dichromate; sodium azide; N,O-bis-(trimethylsilyl)-acetamide; tributylphosphine; trifluoromethane sulfonyl chloride; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; water; methylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1300589-70-1
3',5'-di-O-benzyl-4'-C-(tert-butyldiphenylsilyloxymethyl)-5-methylarabinouridine

: 1300589-85-8
C₂₅H₂₇N₃O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

2.1: sodium azide / N,N-dimethyl-formamide / 48 h / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12.5 h / Inert atmosphere

4.1: dipyridinium dichromate / N,N-dimethyl-formamide / 4.5 h / 20 °C / Inert atmosphere; Molecular sieve

4.2: 1 h

5.1: water; tributylphosphine / tetrahydrofuran / 3.5 h / 20 °C

With pyridine; dipyridinium dichromate; sodium azide; tributylphosphine; tetrabutyl ammonium fluoride; water; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;