C₃₈H₅₁NO₅Si

Base Information

Chemical Name:C₃₈H₅₁NO₅Si
CAS No.:1320210-77-2
Molecular Formula:C₃₈H₅₁NO₅Si
Molecular Weight:629.912
Hs Code.:

C<sub>38</sub>H<sub>51</sub>NO<sub>5</sub>Si

Synonyms:C₃₈H₅₁NO₅Si

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Chemical Property of C₃₈H₅₁NO₅Si

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Technology Process of C₃₈H₅₁NO₅Si

There total 12 articles about C₃₈H₅₁NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 773837-37-9
sodium cyanide

: C₃₇H₅₁IO₅Si

: 1320210-77-2
C₃₈H₅₁NO₅Si

Guidance literature:: In dimethyl sulfoxide; at 70 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: 1320210-70-5
C₂₅H₂₈O₆

: 1320210-77-2
C₃₈H₅₁NO₅Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

2.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

2.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

3.2: Saturated solution

4.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0 °C / Inert atmosphere

4.2: 19 h / 0 - 60 °C / Inert atmosphere

5.1: methanol; 10-camphorsulfonic acid / 24 h / 20 °C / Inert atmosphere

6.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere

7.1: methanol; 10-camphorsulfonic acid / 1 h / 0 °C / Inert atmosphere

8.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 1 h / 40 °C / Inert atmosphere

9.1: dimethyl sulfoxide / 3 h / 70 °C / Inert atmosphere

With 1H-imidazole; titanium(IV) isopropylate; methanol; diethyl (2R,3R)-tartrate; iodine; sodium hydride; diisobutylaluminium hydride; triphenylphosphine; 10-camphorsulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; benzene; 2.1: Sharpless epoxidation / 2.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: C₄₃H₆₆O₆Si₂

: 1320210-77-2
C₃₈H₅₁NO₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; 10-camphorsulfonic acid / 1 h / 0 °C / Inert atmosphere

2: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 1 h / 40 °C / Inert atmosphere

3: dimethyl sulfoxide / 3 h / 70 °C / Inert atmosphere

With 1H-imidazole; methanol; iodine; triphenylphosphine; 10-camphorsulfonic acid; In diethyl ether; dimethyl sulfoxide; benzene;
DOI:10.1016/j.tet.2012.01.071