trans-[Pd(C(=N-2,6-dimethylphenyl)C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(CN-2,6-dimethylphenyl)2]

Base Information

• Chemical Name: trans-[Pd(C(=N-2,6-dimethylphenyl)C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(CN-2,6-dimethylphenyl)2]
• CAS No.: 868158-50-3
• Molecular Formula: C₄₁H₄₀IN₅OPd
• Molecular Weight: 852.126

Synonyms:trans-[Pd(C(=N-2,6-dimethylphenyl)C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(CN-2,6-dimethylphenyl)2]

Chemical Property of trans-[Pd(C(=N-2,6-dimethylphenyl)C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(CN-2,6-dimethylphenyl)2]

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Technology Process of trans-[Pd(C(=N-2,6-dimethylphenyl)C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(CN-2,6-dimethylphenyl)2]

There total 4 articles about trans-[Pd(C(=N-2,6-dimethylphenyl)C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(CN-2,6-dimethylphenyl)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[Pd(C6H4NHC(O)NH(C6H4Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)] (868158-56-9) + 2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) → trans-[Pd(C(=N-2,6-dimethylphenyl)C6H4NHC(O)NH(C6H4Me-4)-2)I(CN-2,6-dimethylphenyl)2] (868158-50-3)

Guidance literature:

In dichloromethane; addn. of isonitrile to a soln. of palladium complex in CH2Cl2, standing for 20 min; concn., addn. of Et2O, filtration, washing with Et2O, drying in air; elem. anal.;

DOI:10.1021/om050451y

Reference yield: 12.0%

trans-[Pd(C6H4NHC(O)NH(C6H4Me-4)-2)I(PPh3)2]*0.17CH2Cl2 + 2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) → trans-[Pd(C(=N-2,6-dimethylphenyl)C6H4NHC(O)NH(C6H4Me-4)-2)I(CN-2,6-dimethylphenyl)2] (868158-50-3)

Guidance literature:

In dichloromethane; react. palladium complex with isonitrile in CH2Cl2; recrystn. (CH2Cl2/n-pentane);

DOI:10.1021/om050451y

Reference yield:

1-(2-iodophenyl)-3-p-tolylurea (710316-98-6) → trans-[Pd(C(=N-2,6-dimethylphenyl)C6H4NHC(O)NH(C6H4Me-4)-2)I(CN-2,6-dimethylphenyl)2] (868158-50-3)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: dichloromethane

In dichloromethane; toluene;

DOI:10.1021/om050451y

upstream raw materials:

[Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

2,6-dimethylphenyl isonitrile

1-(2-iodophenyl)-3-p-tolylurea

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