3-(4-methoxyphenyl)-1-[2-acetoxy-4,6-dimethoxyphenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

Base Information

• Chemical Name: 3-(4-methoxyphenyl)-1-[2-acetoxy-4,6-dimethoxyphenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one
• CAS No.: 1229516-35-1
• Molecular Formula: C₂₀H₂₀O₆
• Molecular Weight: 359.342

Synonyms:3-(4-methoxyphenyl)-1-[2-acetoxy-4,6-dimethoxyphenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

Chemical Property of 3-(4-methoxyphenyl)-1-[2-acetoxy-4,6-dimethoxyphenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(4-methoxyphenyl)-1-[2-acetoxy-4,6-dimethoxyphenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

There total 4 articles about 3-(4-methoxyphenyl)-1-[2-acetoxy-4,6-dimethoxyphenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C15(13)C3H18O5 (1229516-34-0) + acetic anhydride (108-24-7) → 3-(4-methoxyphenyl)-1-[2-acetoxy-4,6-dimethoxyphenyl]-2-[1,2,3-(13)C3]propen-1-one (1229516-35-1)

Guidance literature:

With pyridine; at 20 ℃; for 24h;

DOI:10.1002/jlcr.1732

Reference yield:

(13C)-4-methoxybenzonitrile (1333245-00-3) → 3-(4-methoxyphenyl)-1-[2-acetoxy-4,6-dimethoxyphenyl]-2-[1,2,3-(13)C3]propen-1-one (1229516-35-1)

Guidance literature:

Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 20 °C

2: potassium hydroxide / tetrahydrofuran; methanol / 6 h / Inert atmosphere; Reflux

3: pyridine / 24 h / 20 °C

With pyridine; diisobutylaluminium hydride; potassium hydroxide; In tetrahydrofuran; methanol;

DOI:10.1002/jlcr.1732

Reference yield:

para-iodoanisole (696-62-8) → 3-(4-methoxyphenyl)-1-[2-acetoxy-4,6-dimethoxyphenyl]-2-[1,2,3-(13)C3]propen-1-one (1229516-35-1)

Guidance literature:

Multi-step reaction with 4 steps

1: palladium diacetate; calcium hydroxide / N,N-dimethyl-formamide / 16 h / Reflux

2: diisobutylaluminium hydride / tetrahydrofuran / 20 °C

3: potassium hydroxide / tetrahydrofuran; methanol / 6 h / Inert atmosphere; Reflux

4: pyridine / 24 h / 20 °C

With pyridine; palladium diacetate; diisobutylaluminium hydride; potassium hydroxide; calcium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1002/jlcr.1732

upstream raw materials:

C₁₅⁽¹³⁾C₃H₁₈O₅

acetic anhydride

(¹³C)-4-methoxybenzonitrile

4,6-dimethoxy-2-hydroxy-[1',2'-⁽¹³⁾C]acetophenone

Downstream raw materials:

5,7,4'-trimethoxy-[2,3,4-⁽¹³⁾C₃]isoflavone

[2,3,4-⁽¹³⁾C₃]genistein

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1229516-35-1 3-(4-methoxyphenyl)-1-[2-acetoxy-4,6-dimethoxyphenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

Send

Send

Metric Ton KG G Pound L ML

Send

Send