methyl O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate

Base Information

Chemical Name:methyl O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate
CAS No.:959992-18-8
Molecular Formula:C₁₉H₂₃N₃O₄
Molecular Weight:357.409
Hs Code.:

Synonyms:methyl O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate

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Chemical Property of methyl O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate

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Technology Process of methyl O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate

There total 2 articles about methyl O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 959992-20-2
tert-butyl 6-[2-(4-{(2S)-2-[(tert-butoxycarbonyl)amino]-3-methoxy-3-oxopropyl}phenoxy)ethyl]-2,3-dihydro-4H-pyrido[3,2-b][1,4]oxazin-4-carboxylate

: 959992-18-8
methyl O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate

Guidance literature:: tert-butyl 6-[2-(4-{(2S)-2-[(tert-butoxycarbonyl)amino]-3-methoxy-3-oxopropyl}phenoxy)ethyl]-2,3-dihydro-4H-pyrido[3,2-b][1,4]oxazin-4-carboxylate; With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 12h;

With sodium hydroxide; water;

Reference yield: 80.0%

: methyl O-[2-(4-tert-butoxycarbonyl-3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate

: 959992-18-8
methyl O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate

Guidance literature:: methyl O-[2-(4-tert-butoxycarbonyl-3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate; With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 12h;

With sodium hydroxide; water; In dichloromethane;

Reference yield: 76.0%

: 959992-18-8
methyl O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate

: 1123-25-7
1-methyl-1-cyclohexanecarboxylic acid

: 1041664-31-6
O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-N-[(1-methylcyclohexyl)carbonyl]-L-tyrosine

Guidance literature:: methyl O-[2-(3,4-dihydro-2H-pyrido[3,2-b][1,4]oxazin-6-yl)ethyl]-L-tyrosinate; 1-methyl-1-cyclohexanecarboxylic acid; With 4-methyl-morpholine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; at 30 ℃; for 30h;

With sodium hydroxide; water; In N,N-dimethyl-formamide; at 40 ℃; for 4h;