N-(2-Ethoxycarbonyl-1-cyclohexenyl)-L-valine diallylamide

Base Information

Chemical Name:N-(2-Ethoxycarbonyl-1-cyclohexenyl)-L-valine diallylamide
CAS No.:302800-29-9
Molecular Formula:C₂₀H₃₂N₂O₃
Molecular Weight:348.486
Hs Code.:

Synonyms:N-(2-Ethoxycarbonyl-1-cyclohexenyl)-L-valine diallylamide

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Chemical Property of N-(2-Ethoxycarbonyl-1-cyclohexenyl)-L-valine diallylamide

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Technology Process of N-(2-Ethoxycarbonyl-1-cyclohexenyl)-L-valine diallylamide

There total 4 articles about N-(2-Ethoxycarbonyl-1-cyclohexenyl)-L-valine diallylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1655-07-8
ethyl 2-oxocyclohexane carboxylate

: 302800-22-2
L-valine diallylamide

: 302800-29-9
N-(2-Ethoxycarbonyl-1-cyclohexenyl)-L-valine diallylamide

Guidance literature:: With hydrogenchloride; 4 A molecular sieve; In toluene; at 60 - 65 ℃;
DOI:10.1002/1521-3765(20010302)7:5<1014::AID-CHEM1014>3.0.CO;2-X

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 302800-29-9
N-(2-Ethoxycarbonyl-1-cyclohexenyl)-L-valine diallylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 23 °C

2: 70 percent / trifluoroacetic acid / CH₂Cl₂ / 23 °C

3: 34 percent / aq. HCl; molecular sieves 4 Angstroem / toluene / 60 - 65 °C

With hydrogenchloride; 4 A molecular sieve; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; toluene;
DOI:10.1002/1521-3765(20010302)7:5<1014::AID-CHEM1014>3.0.CO;2-X

Reference yield:

: 72-18-4,25609-85-2,7004-03-7,921-10-8
L-valine

: 302800-29-9
N-(2-Ethoxycarbonyl-1-cyclohexenyl)-L-valine diallylamide

Guidance literature:: Multi-step reaction with 4 steps

1: aq. Na₂CO₃ / methanol / 16 h / 23 °C

2: 93 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 23 °C

3: 70 percent / trifluoroacetic acid / CH₂Cl₂ / 23 °C

4: 34 percent / aq. HCl; molecular sieves 4 Angstroem / toluene / 60 - 65 °C

With hydrogenchloride; 4 A molecular sieve; sodium carbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid; In methanol; dichloromethane; toluene;
DOI:10.1002/1521-3765(20010302)7:5<1014::AID-CHEM1014>3.0.CO;2-X