2,4,6-triethynylbenzenamine

Base Information

• Chemical Name: 2,4,6-triethynylbenzenamine
• CAS No.: 1369583-36-7
• Molecular Formula: C₁₂H₇N
• Molecular Weight: 165.194

Synonyms:2,4,6-triethynylbenzenamine

Chemical Property of 2,4,6-triethynylbenzenamine

Chemical Property:

Purity/Quality:

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Technology Process of 2,4,6-triethynylbenzenamine

There total 2 articles about 2,4,6-triethynylbenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2,4,6-tris((trimethylsilyl)ethynyl)benzenamine → 2,4,6-triethynylbenzenamine (1369583-36-7)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1002/anie.201910588

Reference yield:

2,4,6-triiodoaniline (24154-37-8) → 2,4,6-triethynylbenzenamine (1369583-36-7)

Guidance literature:

Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / tetrahydrofuran / 18 h / 50 °C

2: methanol; potassium hydroxide / tetrahydrofuran

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; potassium hydroxide; In tetrahydrofuran;

DOI:10.1002/chem.201101341

Reference yield:

2,4,6-triethynylbenzenamine (1369583-36-7) + di-tert-butyl 5-azidoisophthalate → C60H70N10O12

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In tetrahydrofuran; water; at 50 ℃; for 72h;

DOI:10.1016/j.inoche.2014.04.027

upstream raw materials:

2,4,6-triiodoaniline

Downstream raw materials:

C₃₆H₁₉NO₁₂

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