[3-(3'7'-dimethyl-2-octen-6'S,7'-diol)-4-(tert-butyldimethyl-siloxy)-5-methoxy-benzyloxy]-tert-butyldimethylsilane

Base Information

• Chemical Name: [3-(3'7'-dimethyl-2-octen-6'S,7'-diol)-4-(tert-butyldimethyl-siloxy)-5-methoxy-benzyloxy]-tert-butyldimethylsilane
• CAS No.: 844868-72-0
• Molecular Formula: C₃₀H₅₆O₅Si₂
• Molecular Weight: 552.943

Synonyms:[3-(3'7'-dimethyl-2-octen-6'S,7'-diol)-4-(tert-butyldimethyl-siloxy)-5-methoxy-benzyloxy]-tert-butyldimethylsilane

Chemical Property of [3-(3'7'-dimethyl-2-octen-6'S,7'-diol)-4-(tert-butyldimethyl-siloxy)-5-methoxy-benzyloxy]-tert-butyldimethylsilane

Chemical Property:

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Technology Process of [3-(3'7'-dimethyl-2-octen-6'S,7'-diol)-4-(tert-butyldimethyl-siloxy)-5-methoxy-benzyloxy]-tert-butyldimethylsilane

There total 3 articles about [3-(3'7'-dimethyl-2-octen-6'S,7'-diol)-4-(tert-butyldimethyl-siloxy)-5-methoxy-benzyloxy]-tert-butyldimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

[4-(tert-butyldimethylsiloxy)-5-methoxy-3-(3',7'-dimethyl-2',6'-octadienyl)benzyloxy]-tert-butyldimethylsilane (474970-89-3) → [3-(3'7'-dimethyl-2-octen-6'S,7'-diol)-4-(tert-butyldimethyl-siloxy)-5-methoxy-benzyloxy]-tert-butyldimethylsilane (844868-72-0)

Guidance literature:

With methanesulfonamide; In water; tert-butyl alcohol; at -7 - 20 ℃; for 140h;

Reference yield: 83.0%

methoxy-phenyl-acetic acid 6-[2-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3-methoxy-phenyl]-1-(1-hydroxy-1-methyl-ethyl)-4-methyl-hex-4-enyl ester (844868-73-1) → [3-(3'7'-dimethyl-2-octen-6'S,7'-diol)-4-(tert-butyldimethyl-siloxy)-5-methoxy-benzyloxy]-tert-butyldimethylsilane (844868-72-0)

Guidance literature:

With sodium hydroxide; In ethanol; water;

DOI:10.1021/jo048444r

Reference yield:

[4-(tert-butyldimethylsiloxy)-5-methoxy-3-(3',7'-dimethyl-2',6'-octadienyl)benzyloxy]-tert-butyldimethylsilane (474970-89-3) → [3-(3'7'-dimethyl-2-octen-6'S,7'-diol)-4-(tert-butyldimethyl-siloxy)-5-methoxy-benzyloxy]-tert-butyldimethylsilane (844868-72-0) + 8-[2-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3-methoxy-phenyl]-2,6-dimethyl-oct-6-ene-2,3-diol (844868-81-1)

Guidance literature:

With AD-mix-α; methanesulfonamide; In water; tert-butyl alcohol; at 6 ℃; for 15h; Title compound not separated from byproducts;

DOI:10.1021/jo048444r

upstream raw materials:

[4-(tert-butyldimethylsiloxy)-5-methoxy-3-(3',7'-dimethyl-2',6'-octadienyl)benzyloxy]-tert-butyldimethylsilane

methoxy-phenyl-acetic acid 6-[2-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3-methoxy-phenyl]-1-(1-hydroxy-1-methyl-ethyl)-4-methyl-hex-4-enyl ester

Downstream raw materials:

methoxy-phenyl-acetic acid 6-[2-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3-methoxy-phenyl]-1-(1-hydroxy-1-methyl-ethyl)-4-methyl-hex-4-enyl ester

7-{2-[4-(8-hydroxy-3,7-dimethylocta-6,7-dienyl)-3,5-bis(methoxymethoxy)phenyl]vinyl}-5-methoxy-1,1,4a-trimethyl-2,3,4,4a,9,9a-hexahydro-1H-xanthen-2-ol

[4-(tert-butyl(dimethyl)silyloxy)-5-methoxy-3-(3',7'-dimethyl-6',7'-epoxy-2'-octenyl)benzyloxy](tert-butyl)(dimethyl)silane

(6'R)-4-hydroxy-3-methoxy-5-(3',7'-dimethyl-6',7'-epoxy-2'-octenyl)benzyl alcohol

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