Technology Process of C25H27N3O5S
There total 6 articles about C25H27N3O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
palladium diacetate; tris-(o-tolyl)phosphine;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 2h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride; potassium iodide; potassium iodate / water / 1 h / 0 - 25 °C
2: tetrahydrofuran / 14 h / 80 °C
3: triethylamine / triphenylphosphine; palladium dichloride / water; tetrahydrofuran / 2 h / 120 °C / Microwave irradiation
4: triethylamine / palladium diacetate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 2 h / 100 °C / Microwave irradiation
With
hydrogenchloride; potassium iodate; triethylamine; potassium iodide;
palladium diacetate; triphenylphosphine; tris-(o-tolyl)phosphine; palladium dichloride;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / 1 h / 0 - 60 °C
2: triethylamine / palladium diacetate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 2 h / 100 °C / Microwave irradiation
With
pyridine; triethylamine;
palladium diacetate; tris-(o-tolyl)phosphine;
In
N,N-dimethyl-formamide;