(S)-<2-2H>-3-methylbut-3-enyl toluene-p-sulphonate

Base Information

Chemical Name:(S)-<2-2H>-3-methylbut-3-enyl toluene-p-sulphonate
CAS No.:117138-03-1
Molecular Formula:C₁₂H₁₆O₃S
Molecular Weight:241.315
Hs Code.:

Synonyms:(S)-<2-2H>-3-methylbut-3-enyl toluene-p-sulphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-<2-2H>-3-methylbut-3-enyl toluene-p-sulphonate

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Technology Process of (S)-<2-2H>-3-methylbut-3-enyl toluene-p-sulphonate

There total 10 articles about (S)-<2-2H>-3-methylbut-3-enyl toluene-p-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 117138-02-0
(R)-<2-2H>-3-hydroxy-3-methylbutyl toluene-p-sulphonate

: 117138-03-1
(S)-<2-2H>-3-methylbut-3-enyl toluene-p-sulphonate

Guidance literature:: With methanesulfonyl chloride; triethylamine; In diethyl ether; 1.) 0 deg C, 1 h; 2.) r.t., 1 h;

Reference yield:

: 477255-00-8
(2S)-[2-²H₁]-isopentenol

: 98-59-9
p-toluenesulfonyl chloride

: 117138-03-1
(S)-<2-2H>-3-methylbut-3-enyl toluene-p-sulphonate

Guidance literature:: With dmap; calcium hydride; In dichloromethane; at 20 ℃;
DOI:10.1021/ol0524050

Reference yield:

: 871325-95-0
tert-butyldimethyl((2S)-3-methyl-2-deuterobut-3-enyloxy)silane

: 117138-03-1
(S)-<2-2H>-3-methylbut-3-enyl toluene-p-sulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

2: calcium hydride; N,N-dimethyl-4-aminopyridine / CH₂Cl₂ / 20 °C

With dmap; calcium hydride; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0524050