(3aR)-1c.4c-dimethyl-7c-(α-hydroxy-isopropyl)-(3arH.8acH)-decahydro-azulene

Base Information

Chemical Name:(3aR)-1c.4c-dimethyl-7c-(α-hydroxy-isopropyl)-(3arH.8acH)-decahydro-azulene
CAS No.:3526-76-9
Molecular Formula:C₁₅H₂₈O
Molecular Weight:224.387
Hs Code.:

(3a<i>R</i>)-1<i>c</i>.4<i>c</i>-dimethyl-7<i>c</i>-(α-hydroxy-isopropyl)-(3a<i>rH</i>.8a<i>cH</i>)-decahydro-azulene

Synonyms:(3aR)-1c.4c-dimethyl-7c-(α-hydroxy-isopropyl)-(3arH.8acH)-decahydro-azulene

Suppliers and Price of (3aR)-1c.4c-dimethyl-7c-(α-hydroxy-isopropyl)-(3arH.8acH)-decahydro-azulene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of (3aR)-1c.4c-dimethyl-7c-(α-hydroxy-isopropyl)-(3arH.8acH)-decahydro-azulene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (3aR)-1c.4c-dimethyl-7c-(α-hydroxy-isopropyl)-(3arH.8acH)-decahydro-azulene

There total 6 articles about (3aR)-1c.4c-dimethyl-7c-(α-hydroxy-isopropyl)-(3arH.8acH)-decahydro-azulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 489-86-1
guaiol

: 3526-76-9
(3aR)-1c.4c-dimethyl-7c-(α-hydroxy-isopropyl)-(3arH.8acH)-decahydro-azulene

: 3526-75-8
(3aS)-1t.4t-dimethyl-7t-(α-hydroxy-isopropyl)-(3arH.8acH)-decahydro-azulene

Guidance literature:: With ethanol; nickel; at 100 ℃; under 73550.8 Torr; Hydrogenation;
DOI:10.1021/ja01499a045 DOI:10.1248/cpb1953.1.241 DOI:10.1002/hlca.194002301115

Reference yield:

: 20482-26-2,33785-03-4,74430-74-3,130796-85-9
liguloxide-3-one

: 3526-75-8,3526-76-9,28892-33-3,46506-69-8
1β,5α-Dihydro-4ξ-guaiol

Guidance literature:: Multi-step reaction with 2 steps

1: Al₂O₃ / petroleum ether

2: (i) H₂, Pd-C, EtOH, (ii) aq. N₂H₄, KOH, triethylene glycol

With aluminum oxide; In Petroleum ether;
DOI:10.1016/S0040-4020(01)92850-9