C₁₄H₁₁BrF₃NO

Base Information

Chemical Name:C₁₄H₁₁BrF₃NO
CAS No.:1128105-72-5
Molecular Formula:C₁₄H₁₁BrF₃NO
Molecular Weight:346.147
Hs Code.:

C<sub>14</sub>H<sub>11</sub>BrF<sub>3</sub>NO

Synonyms:C₁₄H₁₁BrF₃NO

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Chemical Property of C₁₄H₁₁BrF₃NO

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Technology Process of C₁₄H₁₁BrF₃NO

There total 7 articles about C₁₄H₁₁BrF₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1128105-87-2
C₁₄H₁₃BrFNO₂

: 1128105-72-5
C₁₄H₁₁BrF₃NO

Guidance literature:: C₁₄H₁₃BrFNO₂; With Dess-Martin periodane;

With diethylamino-sulfur trifluoride;
DOI:10.1021/ml1000799

Reference yield: 60.0%

: 1128105-71-4
C₁₄H₁₁BrFNO₂

: 1128105-72-5
C₁₄H₁₁BrF₃NO

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ml2000438

Reference yield:

: 1128105-86-1
C₁₅H₁₃BrFNO₃

: 1128105-72-5
C₁₄H₁₁BrF₃NO

Guidance literature:: Multi-step reaction with 5 steps

1: water; sodium hydroxide / methanol / 16 h / 20 °C / Inert atmosphere

2: pyridine; trifluoro-[1,3,5]triazine / dichloromethane / -10 - 20 °C / Inert atmosphere

3: sodium tetrahydroborate / methanol; dichloromethane / 2 h / 20 °C / Inert atmosphere

4: dipyridinium dichromate / dichloromethane / 4 h / 20 °C / Inert atmosphere

5: diethylamino-sulfur trifluoride / dichloromethane / 16 h / 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; dipyridinium dichromate; trifluoro-[1,3,5]triazine; diethylamino-sulfur trifluoride; water; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1021/ml2000438