tert-butyl 3-[3-(4,5-dibromo-6-oxopyridazin-1(6H)-yl)phenoxy]propylcarbamate

Base Information

• Chemical Name: tert-butyl 3-[3-(4,5-dibromo-6-oxopyridazin-1(6H)-yl)phenoxy]propylcarbamate
• CAS No.: 1035451-21-8
• Molecular Formula: C₁₈H₂₁Br₂N₃O₄
• Molecular Weight: 503.19

Synonyms:tert-butyl 3-[3-(4,5-dibromo-6-oxopyridazin-1(6H)-yl)phenoxy]propylcarbamate

Chemical Property of tert-butyl 3-[3-(4,5-dibromo-6-oxopyridazin-1(6H)-yl)phenoxy]propylcarbamate

Chemical Property:

Purity/Quality:

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Technology Process of tert-butyl 3-[3-(4,5-dibromo-6-oxopyridazin-1(6H)-yl)phenoxy]propylcarbamate

There total 1 articles about tert-butyl 3-[3-(4,5-dibromo-6-oxopyridazin-1(6H)-yl)phenoxy]propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H13Br2N3O2 (1035451-66-1) + di-tert-butyl dicarbonate (24424-99-5) → tert-butyl 3-[3-(4,5-dibromo-6-oxopyridazin-1(6H)-yl)phenoxy]propylcarbamate (1035451-21-8)

Guidance literature:

With sodium hydroxide; In water; at 20 ℃; pH=~ 6;

Reference yield: 94.0%

tert-butyl 3-[3-(4,5-dibromo-6-oxopyridazin-1(6H)-yl)phenoxy]propylcarbamate (1035451-21-8) → 2-[3-(3-aminopropoxy)phenyl]-4,5-dibromopyridazin-3(2H)-one hydrochloride (1035451-23-0)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 7h;

upstream raw materials:

C₁₃H₁₃Br₂N₃O₂

di-tert-butyl dicarbonate

Downstream raw materials:

2-[3-(3-aminopropoxy)phenyl]-4,5-dibromopyridazin-3(2H)-one hydrochloride

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