6-<<(3,4-dichlorophenyl)methyl>sulfinyl>-N,N-dimethyl-1,2,4,5-tetrazin-3-amine

Base Information

Chemical Name:6-<<(3,4-dichlorophenyl)methyl>sulfinyl>-N,N-dimethyl-1,2,4,5-tetrazin-3-amine
CAS No.:75328-98-2
Molecular Formula:C₁₁H₁₁Cl₂N₅OS
Molecular Weight:332.213
Hs Code.:

Synonyms:6-<<(3,4-dichlorophenyl)methyl>sulfinyl>-N,N-dimethyl-1,2,4,5-tetrazin-3-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-<<(3,4-dichlorophenyl)methyl>sulfinyl>-N,N-dimethyl-1,2,4,5-tetrazin-3-amine

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Technology Process of 6-<<(3,4-dichlorophenyl)methyl>sulfinyl>-N,N-dimethyl-1,2,4,5-tetrazin-3-amine

There total 3 articles about 6-<<(3,4-dichlorophenyl)methyl>sulfinyl>-N,N-dimethyl-1,2,4,5-tetrazin-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 75328-96-0
6-<<(3,4-dichlorophenyl)methyl>thio>-N,N-dimethyl-1,2,4,5-tetrazin-3-amine

: 75328-98-2
6-<<(3,4-dichlorophenyl)methyl>sulfinyl>-N,N-dimethyl-1,2,4,5-tetrazin-3-amine

Guidance literature:: With Bromine complex of 1,4-diazabicyclo<2.2.2>octane; In water; acetic acid; for 20h; Ambient temperature;
DOI:10.1002/jhet.5570170316

Reference yield:

: 75328-83-5
3,6-bis<<(3,4-dichlorophenyl)methyl>thio>-1,2,4,5-tetrazine

: 75328-98-2
6-<<(3,4-dichlorophenyl)methyl>sulfinyl>-N,N-dimethyl-1,2,4,5-tetrazin-3-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / H₂O; ethanol / 2 h / Heating

2: 83 percent / bromine complex of 1,4-diazabicyclo<2.2.2>octane / H₂O; acetic acid / 20 h / Ambient temperature

With Bromine complex of 1,4-diazabicyclo<2.2.2>octane; In ethanol; water; acetic acid;
DOI:10.1002/jhet.5570170316

Reference yield:

: 75328-82-4
3,6-bis<<(3,4-dichlorophenyl)methyl>thio>-1,2-dihydro-1,2,4,5-tetrazine

: 75328-98-2
6-<<(3,4-dichlorophenyl)methyl>sulfinyl>-N,N-dimethyl-1,2,4,5-tetrazin-3-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / 2N FeCl₃ / ethanol / 1 h

2: 74 percent / H₂O; ethanol / 2 h / Heating

3: 83 percent / bromine complex of 1,4-diazabicyclo<2.2.2>octane / H₂O; acetic acid / 20 h / Ambient temperature

With Bromine complex of 1,4-diazabicyclo<2.2.2>octane; iron(III) chloride; In ethanol; water; acetic acid;
DOI:10.1002/jhet.5570170316