(2R,3R)-4-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidene]-2,3-dimethyl-butyric acid

Base Information

Chemical Name:(2R,3R)-4-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidene]-2,3-dimethyl-butyric acid
CAS No.:83803-24-1
Molecular Formula:C₁₆H₂₈O₂
Molecular Weight:252.397
Hs Code.:

Synonyms:(2R,3R)-4-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidene]-2,3-dimethyl-butyric acid

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Chemical Property of (2R,3R)-4-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidene]-2,3-dimethyl-butyric acid

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Technology Process of (2R,3R)-4-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidene]-2,3-dimethyl-butyric acid

There total 1 articles about (2R,3R)-4-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidene]-2,3-dimethyl-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 83803-23-0
Propionic acid (1S,2S,5R)-2-isopropyl-5-methyl-1-((E)-propenyl)-cyclohexyl ester

: 83803-22-9
(1S,2S,5R)-2-isopropyl-5-methyl-1-{1-propen-1-yl}cyclohexan-1-ol

: 83860-22-4
(2S,3R)-4-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidene]-2,3-dimethyl-butyric acid

: 83803-24-1
(2R,3R)-4-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidene]-2,3-dimethyl-butyric acid

Guidance literature:: With lithium cyclohexylisopropylamide; In tetrahydrofuran; for 5h; -70 deg C to 25 deg C;
DOI:10.1021/jo00148a046

Reference yield:

: 83803-24-1
(2R,3R)-4-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidene]-2,3-dimethyl-butyric acid

: 83803-30-9
tert-Butyl-((R)-2,3-dimethyl-butoxy)-diphenyl-silane

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) O₃, 2.) dimethyl sulfide / 1.) CH₂Cl₂

2: 85 percent / HCl / CHCl₃

3: LiAlH₄

4: imidazole / dimethylformamide

5: 84 percent / W-2 Raney nickel

With 1H-imidazole; hydrogenchloride; lithium aluminium tetrahydride; dimethylsulfide; W-2 Raney nickel; ozone; In chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo00148a046

Reference yield:

: 83803-24-1
(2R,3R)-4-[(2S,5R)-2-Isopropyl-5-methyl-cyclohex-(E)-ylidene]-2,3-dimethyl-butyric acid

: 83803-29-6
tert-Butyl-((2R,3S)-3-[1,3]dithian-2-yl-2-methyl-butoxy)-diphenyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) O₃, 2.) dimethyl sulfide / 1.) CH₂Cl₂

2: 85 percent / HCl / CHCl₃

3: LiAlH₄

4: imidazole / dimethylformamide

With 1H-imidazole; hydrogenchloride; lithium aluminium tetrahydride; dimethylsulfide; ozone; In chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo00148a046