2-(2-(2-(4-benzhydrylpiperazin-1-yl)-2-oxoethoxy)acetamido)-5-bromobenzoic acid sodium salt

Base Information

Chemical Name:2-(2-(2-(4-benzhydrylpiperazin-1-yl)-2-oxoethoxy)acetamido)-5-bromobenzoic acid sodium salt
CAS No.:1103927-14-5
Molecular Formula:C₂₈H₂₇BrN₃O₅*Na
Molecular Weight:588.433
Hs Code.:

Synonyms:2-(2-(2-(4-benzhydrylpiperazin-1-yl)-2-oxoethoxy)acetamido)-5-bromobenzoic acid sodium salt

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Chemical Property of 2-(2-(2-(4-benzhydrylpiperazin-1-yl)-2-oxoethoxy)acetamido)-5-bromobenzoic acid sodium salt

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Technology Process of 2-(2-(2-(4-benzhydrylpiperazin-1-yl)-2-oxoethoxy)acetamido)-5-bromobenzoic acid sodium salt

There total 5 articles about 2-(2-(2-(4-benzhydrylpiperazin-1-yl)-2-oxoethoxy)acetamido)-5-bromobenzoic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1103927-14-5
2-(2-(2-(4-benzhydrylpiperazin-1-yl)-2-oxoethoxy)acetamido)-5-bromobenzoic acid sodium salt

Guidance literature:

Reference yield: 77.0%

: 1103930-17-1
methyl 5-bromo-2-[({2-[4-(diphenylmethyl)piperazin-1-yl]-2-oxoethoxy}acetyl)amino]benzoate

: 1103927-14-5
2-(2-(2-(4-benzhydrylpiperazin-1-yl)-2-oxoethoxy)acetamido)-5-bromobenzoic acid sodium salt

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 60 ℃; for 7h;
DOI:10.1248/cpb.59.215

Reference yield:

: 1103930-14-8
(2-{[4-bromo-2-(methoxycarbonyl)phenyl]amino}-2-oxoethoxy)acetic acid

: 1103927-14-5
2-(2-(2-(4-benzhydrylpiperazin-1-yl)-2-oxoethoxy)acetamido)-5-bromobenzoic acid sodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 1 h / 0 - 20 °C

2: N,N-dimethyl acetamide / 1.5 h / 0 - 20 °C

3: sodium hydroxide / tetrahydrofuran; water / 7 h / 60 °C

With oxalyl dichloride; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl acetamide; water;
DOI:10.1248/cpb.59.215