4-(1,3-Diphenyl-5-thioxo-4,5-dihydro-1H-pyrazol-4-yl)-6-p-tolyl-2H-pyridazine-3-thione

Base Information

Chemical Name:4-(1,3-Diphenyl-5-thioxo-4,5-dihydro-1H-pyrazol-4-yl)-6-p-tolyl-2H-pyridazine-3-thione
CAS No.:147674-97-3
Molecular Formula:C₂₆H₂₀N₄S₂
Molecular Weight:452.604
Hs Code.:

Synonyms:4-(1,3-Diphenyl-5-thioxo-4,5-dihydro-1H-pyrazol-4-yl)-6-p-tolyl-2H-pyridazine-3-thione

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Chemical Property of 4-(1,3-Diphenyl-5-thioxo-4,5-dihydro-1H-pyrazol-4-yl)-6-p-tolyl-2H-pyridazine-3-thione

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Technology Process of 4-(1,3-Diphenyl-5-thioxo-4,5-dihydro-1H-pyrazol-4-yl)-6-p-tolyl-2H-pyridazine-3-thione

There total 4 articles about 4-(1,3-Diphenyl-5-thioxo-4,5-dihydro-1H-pyrazol-4-yl)-6-p-tolyl-2H-pyridazine-3-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 147674-77-9
4-(5-Oxo-1,3-diphenyl-4,5-dihydro-1H-pyrazol-4-yl)-6-p-tolyl-4,5-dihydro-2H-pyridazin-3-one

: 147674-97-3
4-(1,3-Diphenyl-5-thioxo-4,5-dihydro-1H-pyrazol-4-yl)-6-p-tolyl-2H-pyridazine-3-thione

Guidance literature:: With tetraphosphorus decasulfide; In xylene; for 6h; Heating;
DOI:10.1246/bcsj.66.477

Reference yield:

: 20972-36-5,35513-41-8,24849-45-4
4-(p-methylphenyl)-4-oxo-2-butenoic acid

: 147674-97-3
4-(1,3-Diphenyl-5-thioxo-4,5-dihydro-1H-pyrazol-4-yl)-6-p-tolyl-2H-pyridazine-3-thione

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / benzene / 10 h / Heating

2: 83 percent / NH₂NH₂*H₂O / ethanol / Heating

3: 67 percent / P₂S₅ / xylene / 6 h / Heating

With tetraphosphorus decasulfide; hydrazine hydrate; In ethanol; xylene; benzene;
DOI:10.1246/bcsj.66.477

Reference yield:

: 4845-49-2
1,3-diphenyl-5-oxo-4,5-dihydro-1H-pyrazole

: 147674-97-3
4-(1,3-Diphenyl-5-thioxo-4,5-dihydro-1H-pyrazol-4-yl)-6-p-tolyl-2H-pyridazine-3-thione

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / benzene / 10 h / Heating

2: 83 percent / NH₂NH₂*H₂O / ethanol / Heating

3: 67 percent / P₂S₅ / xylene / 6 h / Heating

With tetraphosphorus decasulfide; hydrazine hydrate; In ethanol; xylene; benzene;
DOI:10.1246/bcsj.66.477