3',6'-di-O-acetyl-4'-O-(2'',3'',4'',6''-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranose 1',2'-(allyl 2,6-di-O-benzoyl-α-D-glucopyranosid-3-yl orthoacetate)

Base Information

Chemical Name:3',6'-di-O-acetyl-4'-O-(2'',3'',4'',6''-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranose 1',2'-(allyl 2,6-di-O-benzoyl-α-D-glucopyranosid-3-yl orthoacetate)
CAS No.:227751-12-4
Molecular Formula:C₄₉H₅₈O₂₅
Molecular Weight:1046.98
Hs Code.:

Synonyms:3',6'-di-O-acetyl-4'-O-(2'',3'',4'',6''-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranose 1',2'-(allyl 2,6-di-O-benzoyl-α-D-glucopyranosid-3-yl orthoacetate)

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Chemical Property of 3',6'-di-O-acetyl-4'-O-(2'',3'',4'',6''-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranose 1',2'-(allyl 2,6-di-O-benzoyl-α-D-glucopyranosid-3-yl orthoacetate)

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Technology Process of 3',6'-di-O-acetyl-4'-O-(2'',3'',4'',6''-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranose 1',2'-(allyl 2,6-di-O-benzoyl-α-D-glucopyranosid-3-yl orthoacetate)

There total 1 articles about 3',6'-di-O-acetyl-4'-O-(2'',3'',4'',6''-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranose 1',2'-(allyl 2,6-di-O-benzoyl-α-D-glucopyranosid-3-yl orthoacetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 127446-71-3
Allyl 2,6-di-O-benzoyl-α-D-glucopyranoside

: 4753-07-5,5160-10-1,14206-57-6,14227-66-8,14257-35-3,42385-75-1,67650-37-7,68682-05-3,69308-57-2,69349-74-2,70223-96-0,70223-97-1,71276-38-5,85248-99-3,118493-15-5,120575-76-0
2,3,6,2',3',4',6'-hepta-O-acetyl-α-D-maltosyl bromide

: 227751-12-4
3',6'-di-O-acetyl-4'-O-(2'',3'',4'',6''-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranose 1',2'-(allyl 2,6-di-O-benzoyl-α-D-glucopyranosid-3-yl orthoacetate)

Guidance literature:: With 2,4-lutidine; 4 Angstroem MS; silver trifluoromethanesulfonate; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1080/07328309908544009

Reference yield: 80.0%

: 227751-12-4
3',6'-di-O-acetyl-4'-O-(2'',3'',4'',6''-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranose 1',2'-(allyl 2,6-di-O-benzoyl-α-D-glucopyranosid-3-yl orthoacetate)

: allyl 2,6-di-O-benzoyl-3-O-<2',3',6'-tri-O-acetyl-4'-O-(2'',3'',4'',6''-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosyl>-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 Angstroem MS; In dichloromethane; at -30 ℃; for 0.666667h;
DOI:10.1080/07328309908544009