cycloheptyl-[6-(4-methylsulfanyl-phenyl)-benzo[1,3]dioxol-5-yl]-methanol

Base Information

• Chemical Name: cycloheptyl-[6-(4-methylsulfanyl-phenyl)-benzo[1,3]dioxol-5-yl]-methanol
• CAS No.: 1025912-60-0
• Molecular Formula: C₂₂H₂₆O₃S
• Molecular Weight: 370.513

Synonyms:cycloheptyl-[6-(4-methylsulfanyl-phenyl)-benzo[1,3]dioxol-5-yl]-methanol

Chemical Property of cycloheptyl-[6-(4-methylsulfanyl-phenyl)-benzo[1,3]dioxol-5-yl]-methanol

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of cycloheptyl-[6-(4-methylsulfanyl-phenyl)-benzo[1,3]dioxol-5-yl]-methanol

There total 3 articles about cycloheptyl-[6-(4-methylsulfanyl-phenyl)-benzo[1,3]dioxol-5-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

piperonal (120-57-0,30024-74-9) → cycloheptyl-[6-(4-methylsulfanyl-phenyl)-benzo[1,3]dioxol-5-yl]-methanol (1025912-60-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 70 percent / bromine; acetic acid; iodine / CS₂ / 20 °C

2: 88 percent / sodium carbonate; tetrakis(triphenylphosphine)palladium / ethanol / Heating

3: tetrahydrofuran / 2.17 h / 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; iodine; sodium carbonate; acetic acid; In tetrahydrofuran; carbon disulfide; ethanol; 2: Suzuki coupling / 3: Grignard reaction;

DOI:10.1021/jm030268b

Reference yield:

6-bromo-3,4-methylenedioxybenzaldehyde (15930-53-7) → cycloheptyl-[6-(4-methylsulfanyl-phenyl)-benzo[1,3]dioxol-5-yl]-methanol (1025912-60-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / sodium carbonate; tetrakis(triphenylphosphine)palladium / ethanol / Heating

2: tetrahydrofuran / 2.17 h / 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; ethanol; 1: Suzuki coupling / 2: Grignard reaction;

DOI:10.1021/jm030268b

Reference yield:

cycloheptylmagnesium bromide (78378-12-8) + 6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolane-5-carbaldehyde (445039-73-6) → cycloheptyl-[6-(4-methylsulfanyl-phenyl)-benzo[1,3]dioxol-5-yl]-methanol (1025912-60-0)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃; for 2.16667h;

DOI:10.1021/jm030268b

upstream raw materials:

cycloheptylmagnesium bromide

6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolane-5-carbaldehyde

piperonal

6-bromo-3,4-methylenedioxybenzaldehyde

Downstream raw materials:

cycloheptyl-[6-(4-methanesulfonyl-phenyl)-benzo[1,3]dioxol-5-yl]-methanol

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