8-azidooctyl (3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Base Information

Chemical Name:8-azidooctyl (3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside
CAS No.:1283579-24-7
Molecular Formula:C₆₂H₆₁N₃O₁₇
Molecular Weight:1120.18
Hs Code.:

Synonyms:8-azidooctyl (3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

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Chemical Property of 8-azidooctyl (3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

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Technology Process of 8-azidooctyl (3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

There total 8 articles about 8-azidooctyl (3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1283579-19-0
8-azidooctyl (2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

: 1283579-24-7
8-azidooctyl (3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: With acetyl chloride; In methanol; dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.3762/bjoc.7.47

Reference yield:

: 14218-11-2,14218-30-5,61198-88-7,108438-33-1,108836-02-8,114682-36-9,127305-34-4,151377-77-4
2,3,4,6-Tetra-O-benzoyl-α-D-mannopyranosyl bromide

: 1283579-24-7
8-azidooctyl (3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate; potassium iodide / acetonitrile / Reflux

2: sulfuric acid / 0.5 h / 20 °C

3: ammonium carbonate / N,N-dimethyl-formamide

4: boron trifluoride diethyl etherate / dichloromethane / 2 h / -10 °C / Molecular sieve; Inert atmosphere

5: acetyl chloride / methanol; dichloromethane / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; sulfuric acid; boron trifluoride diethyl etherate; ammonium carbonate; acetyl chloride; potassium iodide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.3762/bjoc.7.47

Reference yield:

: 374078-96-3
1,2-di-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranoside

: 1283579-24-7
8-azidooctyl (3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium carbonate / N,N-dimethyl-formamide

2: boron trifluoride diethyl etherate / dichloromethane / 2 h / -10 °C / Molecular sieve; Inert atmosphere

3: acetyl chloride / methanol; dichloromethane / 0 - 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; ammonium carbonate; acetyl chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3762/bjoc.7.47