phenyl 4-(5-(methylsulfinyl)-4-morpholinopyrimidin-2-yl)phenylcarbamate

Base Information

Chemical Name:phenyl 4-(5-(methylsulfinyl)-4-morpholinopyrimidin-2-yl)phenylcarbamate
CAS No.:1313720-69-2
Molecular Formula:C₂₂H₂₂N₄O₄S
Molecular Weight:438.507
Hs Code.:

Synonyms:phenyl 4-(5-(methylsulfinyl)-4-morpholinopyrimidin-2-yl)phenylcarbamate

Suppliers and Price of phenyl 4-(5-(methylsulfinyl)-4-morpholinopyrimidin-2-yl)phenylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenyl 4-(5-(methylsulfinyl)-4-morpholinopyrimidin-2-yl)phenylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenyl 4-(5-(methylsulfinyl)-4-morpholinopyrimidin-2-yl)phenylcarbamate

There total 5 articles about phenyl 4-(5-(methylsulfinyl)-4-morpholinopyrimidin-2-yl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1313720-37-4
phenyl 4-(5-(methylthio)-4-morpholinopyrimidin-2-yl)phenylcarbamate

: 1313720-69-2
phenyl 4-(5-(methylsulfinyl)-4-morpholinopyrimidin-2-yl)phenylcarbamate

Guidance literature:: phenyl 4-(5-(methylthio)-4-morpholinopyrimidin-2-yl)phenylcarbamate; With dihydrogen peroxide; acetic anhydride; silica gel; In dichloromethane; at 20 ℃;

With sodium hydrogencarbonate; sodium hydrogensulfite; In dichloromethane; water;

Reference yield:

: 7401-98-1
2,4-dichloro-5-methylsulfanylpyrimidine

: 1313720-69-2
phenyl 4-(5-(methylsulfinyl)-4-morpholinopyrimidin-2-yl)phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate / acetone / 1 h / 0 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 12 h / Reflux

3: sodium carbonate / acetonitrile / 8 h / 0 °C

4: acetic anhydride; silica gel; dihydrogen peroxide / dichloromethane / 20 °C

With dihydrogen peroxide; acetic anhydride; silica gel; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water; acetone; acetonitrile;

Reference yield:

: 16350-59-7
5-methylsulfanyl-1H-pyrimidine-2,4-dione

: 1313720-69-2
phenyl 4-(5-(methylsulfinyl)-4-morpholinopyrimidin-2-yl)phenylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: trichlorophosphate; N,N-dimethyl-aniline / 12 h / Reflux

2: sodium carbonate / acetone / 1 h / 0 °C

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 12 h / Reflux

4: sodium carbonate / acetonitrile / 8 h / 0 °C

5: acetic anhydride; silica gel; dihydrogen peroxide / dichloromethane / 20 °C

With dihydrogen peroxide; acetic anhydride; silica gel; sodium carbonate; N,N-dimethyl-aniline; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water; acetone; acetonitrile;